ArticleJACS Au2023
In Situ Multinuclear Magic-Angle Spinning NMR: Monitoring Crystallization of Molecular Sieve AlPO
Article in JACS Au, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Molecular sieves are crystalline three-dimensional frameworks with well-defined channels and cavities. They have been widely used in industry for many applications such as gas separation/purification, ion exchange, and catalysis. Obviously, understanding the formation mechanisms is fundamentally important. High-resolution solid-state NMR spectroscopy is a powerful method for the study of molecular sieves. However, due to technical challenges, the vast majority of the high-resolution solid-state NMR studies on molecular sieve crystallization are ex situ. In the present work, using a new commercially available NMR rotor that can withhold high pressure and high temperature, we examined the formation of molecular sieve AlPO
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