Evidence map›Paper›PMID 37387279›Full record

ArticleSe pu = Chinese journal of chromatography2023

[Determination of bisphenols in sediment by accelerated solvent extraction and solid-phase extraction purification coupled with ultra performance liquid chromatography-tandem mass spectrometry].

Qiu-Xu Wang, Qi-Yan Feng, Xue-Qiang Zhu

Open access · bronzeAbstract readEnglish Abstract
In one paragraph

Article in Se pu = Chinese journal of chromatography, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 6 papers.

0numbers the graph read from it
0cells of the map it votes in
6citing papers in PubMed
0.6field-weighted citation impact, top 35% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

6 citing papers in PubMed, 4 citations in OpenAlex.

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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

3 authors at 1 institution in 1 country.

Qiu-Xu WangSchool of Environment Science and Spatial Informatics, China University of Mining and Technology, Xuzhou 221116, China.
Qi-Yan FengSchool of Environment Science and Spatial Informatics, China University of Mining and Technology, Xuzhou 221116, China.
Xue-Qiang ZhuSchool of Environment Science and Spatial Informatics, China University of Mining and Technology, Xuzhou 221116, China.
China University of Mining and Technology · CN

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Bisphenols are endocrine disruptors that are characterized with bioaccumulation, persistence, and estrogenic activity. Even low contents of bisphenols can exert adverse effects on human health and the ecological environment. Herein, a method combining accelerated solvent extraction and solid-phase extraction purification with ultra performance liquid chromatography-tandem mass spectrometry was developed for the accurate detection of bisphenol A (BPA), bisphenol B (BPB), bisphenol F (BPF), bisphenol S (BPS), bisphenol Z (BPZ), bisphenol AF (BPAF), and bisphenol AP (BPAP) in sediments. The mass spectrometric parameters of the seven bisphenols were optimized, and the response values, separation effects, and chromatographic peak shapes of the target compounds were compared under three different mobile phase conditions. The sediment samples were pretreated by accelerated solvent extraction, and orthogonal tests were used to optimize the extraction solvent, extraction temperature, and cycle number. The results showed that the use of 0.05% (v/v) ammonia and acetonitrile as the mobile phase for gradient elution could rapidly separate the seven bisphenols on an Acquity UPLC BEH C

Indexed as

Tandem Mass SpectrometryAcetonitrilesBisphenol A CompoundsBisphenol B CompoundsBisphenol F CompoundsBisphenol S CompoundsChromatography, LiquidFluorocarbonsHumansacetonitrileAcetonitrilesbisphenol ABisphenol A Compoundsbisphenol AFbisphenol BBisphenol B Compoundsbisphenol FBisphenol F Compoundsbisphenol SBisphenol S CompoundsFluorocarbonsaccelerated solvent extraction (ASE)bisphenolsorthogonal testsedimentsolid-phase extraction (SPE)ultra performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS)

Identifiers

PMID37387279
PMCPMC10311623
OpenAlexW4382631687

What OpenQuestion holds

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LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.