Evidence map›Paper›PMID 37373410›Full record

ArticleInternational journal of molecular sciences2023

First 24-Membered Macrocyclic 1,10-Phenanthroline-2,9-Diamides-An Efficient Switch from Acidic to Alkaline Extraction of

Pavel S Lemport, Valentine S Petrov, Petr I Matveev, Uliana M Leksina, Vitaly A Roznyatovsky, Igor P Gloriozov, Alexandr V Yatsenko, Viktor A Tafeenko, Pavel V Dorovatovskii, Viktor N Khrustalev and 7 more

Abstract read
PubMed Full text at PMC Publisher
In one paragraph

Article in International journal of molecular sciences, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed.

  1. Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

17 authors.

Pavel S LemportDepartment of Chemistry, Lomonosov Moscow State University, Leninskie Gory 1 bld. 3, Moscow 119991, Russia.ORCID 0000-0002-4210-7901
Valentine S PetrovDepartment of Chemistry, Lomonosov Moscow State University, Leninskie Gory 1 bld. 3, Moscow 119991, Russia.
Petr I MatveevDepartment of Chemistry, Lomonosov Moscow State University, Leninskie Gory 1 bld. 3, Moscow 119991, Russia.ORCID 0000-0002-0560-3906
Uliana M LeksinaDepartment of Chemistry, Lomonosov Moscow State University, Leninskie Gory 1 bld. 3, Moscow 119991, Russia.
Vitaly A RoznyatovskyDepartment of Chemistry, Lomonosov Moscow State University, Leninskie Gory 1 bld. 3, Moscow 119991, Russia.ORCID 0000-0002-5673-8931
Igor P GloriozovDepartment of Chemistry, Lomonosov Moscow State University, Leninskie Gory 1 bld. 3, Moscow 119991, Russia.
Alexandr V YatsenkoDepartment of Chemistry, Lomonosov Moscow State University, Leninskie Gory 1 bld. 3, Moscow 119991, Russia.
Viktor A TafeenkoDepartment of Chemistry, Lomonosov Moscow State University, Leninskie Gory 1 bld. 3, Moscow 119991, Russia.
Pavel V DorovatovskiiNational Research Center "Kurchatov Institute", Moscow 123182, Russia.
Viktor N KhrustalevDepartment of Inorganic Chemistry, Peoples' Friendship University of Russia (RUDN University), Moscow 115419, Russia.ORCID 0000-0001-8806-2975
Gleb S BudylinLaboratory of Clinical Biophotonics, Biomedical Science and Technology Park, Sechenov First Moscow State Medical University, Moscow 119991, Russia.
Evgeny A ShirshinLaboratory of Clinical Biophotonics, Biomedical Science and Technology Park, Sechenov First Moscow State Medical University, Moscow 119991, Russia.
Vitaliy Yu MarkovDepartment of Chemistry, Lomonosov Moscow State University, Leninskie Gory 1 bld. 3, Moscow 119991, Russia.ORCID 0000-0003-4452-4087
Alexey A GoryunkovDepartment of Chemistry, Lomonosov Moscow State University, Leninskie Gory 1 bld. 3, Moscow 119991, Russia.ORCID 0000-0003-4460-5370
Vladimir G PetrovDepartment of Chemistry, Lomonosov Moscow State University, Leninskie Gory 1 bld. 3, Moscow 119991, Russia.ORCID 0000-0001-6071-8127
Yuri A UstynyukDepartment of Chemistry, Lomonosov Moscow State University, Leninskie Gory 1 bld. 3, Moscow 119991, Russia.
Valentine G NenajdenkoDepartment of Chemistry, Lomonosov Moscow State University, Leninskie Gory 1 bld. 3, Moscow 119991, Russia.ORCID 0000-0001-9162-5169

Funding

Russian Science Foundation 21-73-10067
6 · The paper itself

Abstract

A reaction of acyl chlorides derived from 1,10-phenanthroline-2,9-dicarboxylic acids with piperazine allows the preparation of the corresponding 24-membered macrocycles in good yield. The structural and spectral properties of these new macrocyclic ligands were thoroughly investigated, revealing promising coordination properties towards f-elements (Am, Eu). It was shown that the prepared ligands can be used for selective extraction of Am(III) from alkaline-carbonate media in presence of Eu(III) with an SF

Indexed as

Coordination ComplexesDiamideLigandsModels, MolecularPhenanthrolines1,10-phenanthrolineCoordination ComplexesDiamideLigandsPhenanthrolinesactinideDFTlanthanidemacrocycleNMRphenanthrolinesolvent extractionXRD

Identifiers

PMID37373410
PMCPMC10299701

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.