ArticleScientific reports2023
Recyclable photocatalyst perovskite as a single-electron redox mediator for visible-light-driven photocatalysis gram-scale synthesis of 3,4-dihydropyrimidin-2-(1H)-ones/thiones in air atmosphere.
Article in Scientific reports, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 6 papers.
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6 citing papers in PubMed.
- Methyl Viologen Lead Iodide for Photocatalytic Reductive Coupling of Aromatic Carbonyls via Proton-Coupled Electron Transfer.ACS applied materials & interfaces · 2026Article
- Halide Perovskite Photocatalysts for Clean Fuel Production and Organic Synthesis: Opportunities and Challenges.Advanced materials (Deerfield Beach, Fla.) · 2025Review
- Magnetic BiFeOScientific reports · 2024Article
- Recent progress of metal halide perovskite materials in heterogeneous photocatalytic organic reactions.Photochemical & photobiological sciences : Official journal of the European Photochemistry Association and the European Society for Photobiology · 2024Review
- Photocatalytic systems: reactions, mechanism, and applications.RSC advances · 2024Review
- O,S,Se-containing Biginelli products based on cyclic β-ketosulfone and their postfunctionalization.Beilstein journal of organic chemistry · 2024Article
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Abstract
Based on the Biginelli reaction of β-ketoesters, arylaldehydes, and urea/thiourea, we created a green radical synthesis procedure for 3,4-dihydropyrimidin-2-(1H)-ones/thiones. A single-electron redox mediator was applied to a solution of ethanol in an air environment, at room temperature, and with blue LEDs as a renewable energy source in order to create. The objective of this research is to create a halide perovskite that is widely available, affordable, recyclable, and economically feasible. A factor mentioned in the discussion is that the procedure tolerates a variety of donating and withdrawing functional groups while still offering a very fast rate and excellent yields. The range of yields is quite uniform (86-94%, average: 90.4%), and the range of reaction times is very quick (4-8 min, average: 5.8 min). Furthermore, gram-scale cyclization shows that it is applicable for use in industry. Additionally, CsPbBr
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