ArticleACS omega2023
Optimization of the Poly(glycerol citraconate) Synthesis Using the Box-Behnken Design.
Article in ACS omega, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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4 authors.
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Abstract
This work aimed to obtain poly(glycerol citraconate) (PGCitrn) for biomedical applications, analyze the obtained polyester by spectroscopic methods, and optimize its preparation. Polycondensation reactions of glycerol and citraconic anhydride were carried out. It was provided that the results in the reaction are oligomers of poly(glycerol citraconate). Optimization studies were carried out based on the Box-Behnken design. The input variables in this plan were the ratio of functional groups, temperature, and time and occurrence in coded form: -1, 0, or 1. Three output variables were optimized: the degree of esterification, the percentage of
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