ArticleNanomaterials (Basel, Switzerland)2023
Radiolysis-Assisted Direct Growth of Gold-Based Electrocatalysts for Glycerol Oxidation.
Article in Nanomaterials (Basel, Switzerland), 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.
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Who cites it
2 citing papers in PubMed, 8 citations in OpenAlex.
- Gold-Indium Electrocatalysts for the Selective Oxidation of Glycerol Coupled with COChemSusChem · 2025Article
- Synthesis of Metallic Nanostructures Using Ionizing Radiation and Their Applications.Materials (Basel, Switzerland) · 2024Review
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Authors and funding
8 authors at 2 institutions in 1 country.
Funding
Abstract
The electrocatalytic oxidation of glycerol by metal electrocatalysts is an effective method of low-energy-input hydrogen production in membrane reactors in alkaline conditions. The aim of the present study is to examine the proof of concept for the gamma-radiolysis-assisted direct growth of monometallic gold and bimetallic gold-silver nanostructured particles. We revised the gamma radiolysis procedure to generate free-standing Au and Au-Ag nano- and micro-structured particles onto a gas diffusion electrode by the immersion of the substrate in the reaction mixture. The metal particles were synthesized by radiolysis on a flat carbon paper in the presence of capping agents. We have integrated different methods (SEM, EDX, XPS, XRD, ICP-OES, CV, and EIS) to examine in detail the as-synthesized materials and interrogate their electrocatalytic efficiency for glycerol oxidation under baseline conditions to establish a structure-performance relationship. The developed strategy can be easily extended to the synthesis by radiolysis of other types of ready-to-use metal electrocatalysts as advanced electrode materials for heterogeneous catalysis.
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Registered trials
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