Evidence map›Paper›PMID 37284256›Full record

ArticleJournal of applied crystallography2023

A reactor for time-resolved X-ray studies of nucleation and growth during solvothermal synthesis.

Martin Roelsgaard, Magnus Kløve, Rasmus Christensen, Andreas D Bertelsen, Nils L N Broge, Innokenty Kantor, Daniel Risskov Sørensen, Ann-Christin Dippel, Soham Banerjee, Martin V Zimmermann and 4 more

Abstract read
In one paragraph

Article in Journal of applied crystallography, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 7 papers.

0numbers the graph read from it
0cells of the map it votes in
7citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

7 citing papers in PubMed.

  1. Article
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  5. Reliability of pair distribution function analysis inJournal of applied crystallography · 2025
    Article
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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

14 authors.

Martin RoelsgaardDepartment of Chemistry and iNANO, Aarhus University, Langelandsgade 140, 8000 Aarhus C, Denmark.ORCID https://orcid.org/0000-0002-0365-3977
Magnus KløveDepartment of Chemistry and iNANO, Aarhus University, Langelandsgade 140, 8000 Aarhus C, Denmark.ORCID https://orcid.org/0000-0001-9513-8798
Rasmus ChristensenDepartment of Chemistry and iNANO, Aarhus University, Langelandsgade 140, 8000 Aarhus C, Denmark.
Andreas D BertelsenDepartment of Chemistry and iNANO, Aarhus University, Langelandsgade 140, 8000 Aarhus C, Denmark.
Nils L N BrogeDepartment of Chemistry and iNANO, Aarhus University, Langelandsgade 140, 8000 Aarhus C, Denmark.
Innokenty KantorMAX IV Laboratory, Lund University, 224 84 Lund, Sweden.ORCID https://orcid.org/0000-0001-5132-8354
Daniel Risskov SørensenDepartment of Chemistry and iNANO, Aarhus University, Langelandsgade 140, 8000 Aarhus C, Denmark.
Ann-Christin DippelDeutsches Elektronen-Synchrotron DESY, Notkestraße 85, 22607 Hamburg, Germany.ORCID https://orcid.org/0000-0003-1735-9215
Soham BanerjeeDeutsches Elektronen-Synchrotron DESY, Notkestraße 85, 22607 Hamburg, Germany.ORCID https://orcid.org/0000-0001-9271-493X
Martin V ZimmermannDeutsches Elektronen-Synchrotron DESY, Notkestraße 85, 22607 Hamburg, Germany.
Philipp GlaeveckeDeutsches Elektronen-Synchrotron DESY, Notkestraße 85, 22607 Hamburg, Germany.
Olof GutowskiDeutsches Elektronen-Synchrotron DESY, Notkestraße 85, 22607 Hamburg, Germany.
Mads Ry Vogel JørgensenDepartment of Chemistry and iNANO, Aarhus University, Langelandsgade 140, 8000 Aarhus C, Denmark.ORCID https://orcid.org/0000-0001-5507-9615
Bo Brummerstedt IversenDepartment of Chemistry and iNANO, Aarhus University, Langelandsgade 140, 8000 Aarhus C, Denmark.ORCID https://orcid.org/0000-0002-4632-1024

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Understanding the nucleation and growth mechanisms of nanocrystals under hydro- and solvothermal conditions is key to tailoring functional nanomaterials. High-energy and high-flux synchrotron radiation is ideal for characterization by powder X-ray diffraction and X-ray total scattering in real time. Different versions of batch-type cell reactors have been employed in this work, exploiting the robustness of polyimide-coated fused quartz tubes with an inner diameter of 0.7 mm, as they can withstand pressures up to 250 bar and temperatures up to 723 K for several hours. Reported here are recent developments of the

Indexed as

in situ X-ray scatteringpowder X-ray diffractionsmall-angle scatteringsolvothermal chemistrytotal scattering

Identifiers

PMID37284256
PMCPMC10241040

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.