Evidence map›Paper›PMID 37237027›Full record

ReviewNature protocols2023

Solution-state nuclear magnetic resonance spectroscopy of crystalline cellulosic materials using a direct dissolution ionic liquid electrolyte.

Lukas Fliri, Katja Heise, Tetyana Koso, Aleksandar R Todorov, Daniel Rico Del Cerro, Sami Hietala, Juha Fiskari, Ilkka Kilpeläinen, Michael Hummel, Alistair W T King

Open access · bronzeAbstract readReview
PubMed Publisher
In one paragraph

Review in Nature protocols, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 11 papers.

0numbers the graph read from it
0cells of the map it votes in
11citing papers in PubMed
6.7field-weighted citation impact, top 2% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

11 citing papers in PubMed, 67 citations in OpenAlex.

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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

10 authors at 3 institutions in 2 countries.

Lukas FliriDepartment of Bioproducts and Biosystems, Aalto University, Espoo, Finland.ORCID 0000-0001-5555-8659
Katja HeiseDepartment of Bioproducts and Biosystems, Aalto University, Espoo, Finland.
Tetyana KosoMaterials Chemistry Division, Department of Chemistry, University of Helsinki, Helsinki, Finland.ORCID 0000-0002-0429-3205
Aleksandar R TodorovMaterials Chemistry Division, Department of Chemistry, University of Helsinki, Helsinki, Finland.ORCID 0000-0001-9147-4874
Daniel Rico Del CerroMaterials Chemistry Division, Department of Chemistry, University of Helsinki, Helsinki, Finland.
Sami HietalaMaterials Chemistry Division, Department of Chemistry, University of Helsinki, Helsinki, Finland.
Juha FiskariFibre Science and Communication Network (FSCN), Mid Sweden University, Sundsvall, Sweden.
Ilkka KilpeläinenMaterials Chemistry Division, Department of Chemistry, University of Helsinki, Helsinki, Finland.
Michael HummelDepartment of Bioproducts and Biosystems, Aalto University, Espoo, Finland. michael.hummel@aalto.fi.
Alistair W T KingMaterials Chemistry Division, Department of Chemistry, University of Helsinki, Helsinki, Finland. alistair.king@vtt.fi.ORCID 0000-0003-3142-9259
University of Helsinki · FIAalto University · FIMid Sweden University · SE

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Owing to its high sustainable production capacity, cellulose represents a valuable feedstock for the development of more sustainable alternatives to currently used fossil fuel-based materials. Chemical analysis of cellulose remains challenging, and analytical techniques have not advanced as fast as the development of the proposed materials science applications. Crystalline cellulosic materials are insoluble in most solvents, which restricts direct analytical techniques to lower-resolution solid-state spectroscopy, destructive indirect procedures or to 'old-school' derivatization protocols. While investigating their use for biomass valorization, tetralkylphosphonium ionic liquids (ILs) exhibited advantageous properties for direct solution-state nuclear magnetic resonance (NMR) analysis of crystalline cellulose. After screening and optimization, the IL tetra-n-butylphosphonium acetate [P

Indexed as

Ionic LiquidsCelluloseElectrolytesMagnetic Resonance SpectroscopySolubilitySolventsCelluloseElectrolytesIonic LiquidsSolvents

Identifiers

PMID37237027
OpenAlexW4378416910

What OpenQuestion holds

Textmetadata
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.