Evidence map›Paper›PMID 37224586›Full record

ArticleJournal of magnetic resonance (San Diego, Calif. : 1997)2023

Diamond rotors.

Natalie C Golota, Zachary P Fredin, Daniel P Banks, David Preiss, Salima Bahri, Prashant Patil, William K Langford, Camron L Blackburn, Erik Strand, Brian Michael and 4 more

Abstract read
In one paragraph

Article in Journal of magnetic resonance (San Diego, Calif. : 1997), 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 6 papers.

0numbers the graph read from it
0cells of the map it votes in
6citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

6 citing papers in PubMed.

  1. Diamond rotors for high magic angle spinning frequencies.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2025
    Article
  2. Dynamic Nuclear Polarization with P1 Centers in Diamond.The journal of physical chemistry letters · 2024
    Article
  3. Characterization of dielectric properties and their impact on MAS-DNP NMR applications.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2024
    Article
  4. Article
  5. High aspect ratio diamond nanosecond laser machining.Applied physics. A, Materials science & processing · 2023
    Article
  6. Additive fabrication for NMR probe builders.Progress in nuclear magnetic resonance spectroscopy
    Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

14 authors.

Natalie C GolotaDepartment of Chemistry, Massachusetts Institute of Technology, Cambridge, MA 02139, USA; Francis Bitter Magnet Laboratory, Massachusetts Institute of Technology, Cambridge, MA 02139, USA.
Zachary P FredinCenter for Bits and Atoms, Massachusetts Institute of Technology, Cambridge, MA 02139, USA.
Daniel P BanksDepartment of Chemistry, Massachusetts Institute of Technology, Cambridge, MA 02139, USA; Francis Bitter Magnet Laboratory, Massachusetts Institute of Technology, Cambridge, MA 02139, USA.
David PreissCenter for Bits and Atoms, Massachusetts Institute of Technology, Cambridge, MA 02139, USA.
Salima BahriDepartment of Chemistry, Massachusetts Institute of Technology, Cambridge, MA 02139, USA; Francis Bitter Magnet Laboratory, Massachusetts Institute of Technology, Cambridge, MA 02139, USA.
Prashant PatilCenter for Bits and Atoms, Massachusetts Institute of Technology, Cambridge, MA 02139, USA.
William K LangfordCenter for Bits and Atoms, Massachusetts Institute of Technology, Cambridge, MA 02139, USA.
Camron L BlackburnCenter for Bits and Atoms, Massachusetts Institute of Technology, Cambridge, MA 02139, USA.
Erik StrandCenter for Bits and Atoms, Massachusetts Institute of Technology, Cambridge, MA 02139, USA.
Brian MichaelDepartment of Chemistry, Massachusetts Institute of Technology, Cambridge, MA 02139, USA; Francis Bitter Magnet Laboratory, Massachusetts Institute of Technology, Cambridge, MA 02139, USA.
Blake DastrupDepartment of Chemistry, Massachusetts Institute of Technology, Cambridge, MA 02139, USA.
Keith A NelsonDepartment of Chemistry, Massachusetts Institute of Technology, Cambridge, MA 02139, USA.
Neil GershenfeldCenter for Bits and Atoms, Massachusetts Institute of Technology, Cambridge, MA 02139, USA.
Robert GriffinDepartment of Chemistry, Massachusetts Institute of Technology, Cambridge, MA 02139, USA; Francis Bitter Magnet Laboratory, Massachusetts Institute of Technology, Cambridge, MA 02139, USA. Electronic address: rgg@mit.edu.

Funding

High Field DNP and EPR in Biological SystemsR01GM132997 · NIGMS · MASSACHUSETTS INSTITUTE OF TECHNOLOGY · PI GRIFFIN, ROBERT GUY · 2019 to 2025
$4.6M
TR&D 4 -- Advanced Magic Angle Spinning NMR methodsP41GM132079 · NIGMS · MASSACHUSETTS INSTITUTE OF TECHNOLOGY · PI GRIFFIN, ROBERT GUY · 2019 to 2021
$3.6M
Solid State NMR Studies of Amyloid ProteinsR01AG058504 · NIA · MASSACHUSETTS INSTITUTE OF TECHNOLOGY · PI ROBERT Guy GRIFFIN · 2022 to 2026
$3.5M
Solid State NMR Studies of Amyloid ProteinsRF1AG058504 · NIA · MASSACHUSETTS INSTITUTE OF TECHNOLOGY · PI GRIFFIN, ROBERT GUY · 2017 to 2017
$3.1M
Diamond RotorsR01GM139055 · NIGMS · MASSACHUSETTS INSTITUTE OF TECHNOLOGY · PI Neil Gershenfeld · 2021 to 2026
$1.7M
NIA NIH HHS R01 AG058504NIA NIH HHS RF1 AG058504NIGMS NIH HHS P41 GM132079NIGMS NIH HHS R01 GM132997NIGMS NIH HHS R01 GM139055
6 · The paper itself

Abstract

The resolution of magic angle spinning (MAS) nuclear magnetic resonance (NMR) spectra remains bounded by the spinning frequency, which is limited by the material strength of MAS rotors. Since diamond is capable of withstanding 1.5-2.5x greater MAS frequencies, compared to state-of-the art zirconia, we fabricated rotors from single crystal diamond. When combined with bearings optimized for spinning with helium gas, diamond rotors could achieve the highest MAS frequencies to date. Furthermore, the excellent microwave transmission properties and thermal conductivity of diamond could improve sensitivity enhancements in dynamic nuclear polarization (DNP) experiments. The fabrication protocol we report involves novel laser micromachining and produced rotors that presently spin at ω

Indexed as

DiamondMicrowavesMagnetic Resonance SpectroscopyProteinsDiamondProteinsDiamond rotorsHigh frequency spinningLaser machiningMagic angle spinning

Identifiers

PMID37224586
PMCPMC10504678

What OpenQuestion holds

Textmetadata
LicenceTDM
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.