Evidence map›Paper›PMID 37125223›Full record

ArticleDesigned monomers and polymers2023

Synthesis and structural characterization of β -cyclodextrin butenate.

Yong-Fu Li, Zhu-Xi Tian, Bin Shi, Yang-Bo He, Ming-Xiu Long

Abstract read
In one paragraph

Article in Designed monomers and polymers, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Review
  2. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

5 authors.

Yong-Fu LiIntegrated Rural Development Center, Guizhou Academy of Agricultural Science, Guiyang, Guizhou, China.
Zhu-Xi TianIntegrated Rural Development Center, Guizhou Academy of Agricultural Science, Guiyang, Guizhou, China.
Bin ShiIntegrated Rural Development Center, Guizhou Academy of Agricultural Science, Guiyang, Guizhou, China.
Yang-Bo HeIntegrated Rural Development Center, Guizhou Academy of Agricultural Science, Guiyang, Guizhou, China.
Ming-Xiu LongIntegrated Rural Development Center, Guizhou Academy of Agricultural Science, Guiyang, Guizhou, China.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

β-cyclodextrin butenate was synthesized by using N, N'-Carbonyldiimidazole (CDI) activating reagent and 4-Dimethylaminopyridine (DMAP) as catalyst. The best preparation condition of β-CD butenate was described as below: reaction temperature was 25°C, concentration of 2-butenoic acid was 450 mmol/L, concentration of DMAP was 12.5 mmol/L and reaction time was 20 minutes and at this condition the yield of β-CD butenate was 0.83 mmol/g. According to the results of FT-IR spectrum, NMR spectroscopy and HPLC-QTof-mass spectrum of β-CD butenate, there were four types β-CD butenate synthesized, which were β-CD-2-butenoic acid monoester, β-CD-2-butenoic acid diester, β-CD-2-butenoic acid triester and β-CD-2-butenoic acid tetraester, respectively.

Indexed as

esterificationN, N’-carbonyldiimidazoleΒ-cyclodextrinβ-cyclodextrin butenate

Identifiers

PMID37125223
PMCPMC10142337

What OpenQuestion holds

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.