ArticleACS nano2023
An Amorphous Phase Precedes Crystallization: Unraveling the Colloidal Synthesis of Zirconium Oxide Nanocrystals.
Article in ACS nano, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 12 papers.
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Who cites it
12 citing papers in PubMed, 24 citations in OpenAlex.
- Decoding α-MoCSmall (Weinheim an der Bergstrasse, Germany) · 2026Article
- Milling-Induced Defects in Ni/Zirconia Catalysts for Enhancing Catalytic Activity in Dry Methane Reforming.The journal of physical chemistry. C, Nanomaterials and interfaces · 2026Article
- Prospects of Nanoscience with Nanocrystals: 2025 Edition.ACS nano · 2025Review
- From Kinetics to Molecular-Level Insights into Group 4 Metal Oxide Nanocrystal Synthesis.ACS materials Au · 2025Article
- Local orthorhombic phase in zirconium oxide nanocrystals: insights from X-ray pair distribution function analysis.Journal of applied crystallography · 2025Article
- Characterization and calibration of DECTRIS PILATUS3 X CdTe 2M high-Journal of applied crystallography · 2025Article
- Epitaxial Core/Shell Nanocrystals of (Europium-Doped) Zirconia and Hafnia.Journal of the American Chemical Society · 2024Article
- Synthesis of zirconium(IV) and hafnium(IV) isopropoxide,Dalton transactions (Cambridge, England : 2003) · 2024Article
- Complexation and disproportionation of group 4 metal (alkoxy) halides with phosphine oxides.Dalton transactions (Cambridge, England : 2003) · 2024Article
- From Gel to Crystal: Mechanism of HfOJournal of the American Chemical Society · 2024Article
- The Chemistry of Spinel Ferrite Nanoparticle Nucleation, Crystallization, and Growth.ACS nano · 2024Article
- Tailoring of Colloidal HfOSmall science · 2024Article
Corrections and comments
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Authors and funding
14 authors at 6 institutions in 5 countries.
Funding
No grant is acknowledged in the PubMed record.
Abstract
One can nowadays readily generate monodisperse colloidal nanocrystals, but the underlying mechanism of nucleation and growth is still a matter of intense debate. Here, we combine X-ray pair distribution function (PDF) analysis, small-angle X-ray scattering (SAXS), nuclear magnetic resonance (NMR), and transmission electron microscopy (TEM) to investigate the nucleation and growth of zirconia nanocrystals from zirconium chloride and zirconium isopropoxide at 340 °C, in the presence of surfactant (tri-
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