Evidence map›Paper›PMID 37040083›Full record

ArticleJournal of the American Chemical Society2023

Catching a New Zeolite as a Transition Material during Deconstruction.

Qiudi Yue, Gwladys Steciuk, Michal Mazur, Jin Zhang, Oleg Petrov, Mariya Shamzhy, Mingxiu Liu, Lukáš Palatinus, Jiří Čejka, Maksym Opanasenko

Abstract read
In one paragraph

Article in Journal of the American Chemical Society, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Review
  2. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

10 authors.

Qiudi YueDepartment of Physical and Macromolecular Chemistry, Faculty of Science, Charles University, Hlavova 8, Prague 2 128 43, Czech Republic.ORCID 0000-0003-2046-5238
Gwladys SteciukInstitute of Physics, Academy of Sciences of the Czech Republic, v.v.i., Na Slovance 2, Prague 8 182 21, Czech Republic.ORCID 0000-0002-5666-3570
Michal MazurDepartment of Physical and Macromolecular Chemistry, Faculty of Science, Charles University, Hlavova 8, Prague 2 128 43, Czech Republic.ORCID 0000-0001-5044-5284
Jin ZhangDepartment of Physical and Macromolecular Chemistry, Faculty of Science, Charles University, Hlavova 8, Prague 2 128 43, Czech Republic.
Oleg PetrovDepartment of Low-Temperature Physics, Faculty of Mathematics and Physics, Charles University, V Holešovičkách 2, Prague 8 180 00, Czech Republic.ORCID 0000-0003-1728-6896
Mariya ShamzhyDepartment of Physical and Macromolecular Chemistry, Faculty of Science, Charles University, Hlavova 8, Prague 2 128 43, Czech Republic.ORCID 0000-0002-1979-6817
Mingxiu LiuDepartment of Physical and Macromolecular Chemistry, Faculty of Science, Charles University, Hlavova 8, Prague 2 128 43, Czech Republic.
Lukáš PalatinusInstitute of Physics, Academy of Sciences of the Czech Republic, v.v.i., Na Slovance 2, Prague 8 182 21, Czech Republic.ORCID 0000-0002-8987-8164
Jiří ČejkaDepartment of Physical and Macromolecular Chemistry, Faculty of Science, Charles University, Hlavova 8, Prague 2 128 43, Czech Republic.ORCID 0000-0003-1400-1031
Maksym OpanasenkoDepartment of Physical and Macromolecular Chemistry, Faculty of Science, Charles University, Hlavova 8, Prague 2 128 43, Czech Republic.ORCID 0000-0002-0833-8255

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Zeolites are key materials in both basic research and industrial applications. However, their synthesis is neither diverse nor applicable to labile frameworks because classical procedures require harsh hydrothermal conditions, whereas post-synthesis methods are limited to a few suitable parent materials. Remaining frameworks can fail due to amorphization, dissolution, and other decomposition processes. Nevertheless, stopping degradation at intermediate structures could yield new zeolites. Here, by optimizing the design and synthesis parameters of the parent zeolite IWV, we "caught" a new, highly crystalline, and siliceous zeolite during its degradation. IWV seed-assisted crystallization followed by gentle transformation into the water-alcohol system yielded the highly crystalline daughter zeolite IPC-20, whose structure was solved by precession-assisted three-dimensional electron diffraction. Without additional requirements, as in conventional (direct or post-synthesis) strategies, our approach may be applied to any chemically labile material with a staged structure.

Identifiers

PMID37040083
PMCPMC10141410

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.