Evidence map›Paper›PMID 37014685›Full record

ArticleArhiv za higijenu rada i toksikologiju2023

How different microfilters affect the recovery of eleven EU-regulated mycotoxins.

Marija Kovač Tomas, Anto Mijatović, Mateja Bulaić Nevistić, Bojan Šarkanj, Jurislav Babić, Tihomir Kovač

Abstract read
In one paragraph

Article in Arhiv za higijenu rada i toksikologiju, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Toxins · 2026
    Review
  2. Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors.

Marija Kovač TomasUniversity North, Department of Food Technology, Koprivnica, Croatia.
Anto MijatovićUniversity North, Department of Food Technology, Koprivnica, Croatia.
Mateja Bulaić NevistićInspecto Ltd., Osijek, Croatia.
Bojan ŠarkanjUniversity North, Department of Food Technology, Koprivnica, Croatia.
Jurislav BabićJosip Juraj Strossmayer University of Osijek, Faculty of Food Technology, Osijek, Croatia.
Tihomir KovačJosip Juraj Strossmayer University of Osijek, Faculty of Food Technology, Osijek, Croatia.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Microfiltration is a common step in liquid chromatography - tandem mass spectrometry (LC-MS), a method of choice in determining several mycotoxins in a solution at once. However, microfiltration may entail filter-analyte interactions that can affect the accuracy of the procedure, and underestimate exposure. The aim of our study was to assess how five different membrane materials for syringe filters (nylon, polytetrafluoroethylene, polyethersulphone, mixed cellulose ester, and cellulose acetate) affect microfiltration and recovery of EU-regulated mycotoxins, including aflatoxins B1, B2, G1, and G2, deoxynivalenol, fumonisins B1 and B2, zearalenone, T-2 and HT-2 toxins, and ochratoxin A. Polytetrafluoroethylene filters turned out to least affect microfiltration through mycotoxin loss, followed by more commonly used nylon filters, whereas the remaining three filter membrane materials had such a negative effect on recoveries that we found them incompatible with the procedure. Our findings clearly suggest that it is important to select a proper filter type that suits analyte properties and solution composition and to discard the first few filtrate drops to ensure the accuracy of the analytical procedure.

Indexed as

MycotoxinsZearalenoneChromatography, High Pressure LiquidChromatography, LiquidNylonsTandem Mass SpectrometryMycotoxinsNylonsZearalenonefilter-analyte interactioninterakcije filtar-analitliquid chromatography-tandem mass spectrometrypodcjenjivanje rezultatapriprema uzorkaregulirani mikotoksinisample preparationtekućinska kromatografija – tandemska spektrometrija masaunderestimation

Identifiers

PMID37014685
PMCPMC10231880

What OpenQuestion holds

Textmetadata
LicenceCC BY-NC-ND
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.