Evidence map›Paper›PMID 36926270›Full record

ArticleMethodsX2023

HRMS-Targeted-DIA methodology for quantification of wastewater-borne pollutants in surface water.

Olga Gómez-Navarro, Francesc Labad, Diana P Manjarrés-López, Sandra Pérez, Nicola Montemurro

Open access · goldFull text read
In one paragraph

Article in MethodsX, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 3 papers.

0numbers the graph read from it
0cells of the map it votes in
3citing papers in PubMed
2.5field-weighted citation impact, top 12% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

3 citing papers in PubMed, 17 citations in OpenAlex.

  1. Article
  2. Article
  3. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

5 authors at 1 institution in 1 country.

Olga Gómez-NavarroONHEALTH, Department of Environmental Chemistry, Institute of Environmental Assessment and Water Research (IDAEA-CSIC), Jordi Girona 18-26, Barcelona 08034, Spain.
Francesc LabadONHEALTH, Department of Environmental Chemistry, Institute of Environmental Assessment and Water Research (IDAEA-CSIC), Jordi Girona 18-26, Barcelona 08034, Spain.
Diana P Manjarrés-LópezONHEALTH, Department of Environmental Chemistry, Institute of Environmental Assessment and Water Research (IDAEA-CSIC), Jordi Girona 18-26, Barcelona 08034, Spain.
Sandra PérezONHEALTH, Department of Environmental Chemistry, Institute of Environmental Assessment and Water Research (IDAEA-CSIC), Jordi Girona 18-26, Barcelona 08034, Spain.
Nicola MontemurroONHEALTH, Department of Environmental Chemistry, Institute of Environmental Assessment and Water Research (IDAEA-CSIC), Jordi Girona 18-26, Barcelona 08034, Spain.
Institute of Environmental Assessment and Water Research · ES

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

A robust method was developed for the quantification of popular and highly occurrence contaminants of emerging concern from wastewater treatment plant effluents and is explained in detail. A homemade multi-layered and multi-sorbent solid phase extraction (SPE) cartridge was used to cover the wide range of polarities of the selected contaminants. A non-discriminant elution protocol was also applied. Liquid chromatography coupled to a high-resolution mass spectrometer (HRMS) Q-Exactive Orbitrap system was used for the separation and detection of the contaminants. A targeted data independent acquisition (DIA) mode with an inclusion list with the exact mass, retention time window and collision energy was tried for the first time obtaining good sensitivity, selectivity and high quality MS2 product ions.•116 compounds of a wide-scope of polarities and physic-chemical properties were validated using a surface water pool matrix.•SPE followed by LC-HRMS with a targeted DIA was used for the method validation at three concentration levels 5, 50, 500 μg l

Indexed as

CECs targeted method for surface waterContaminants of emerging concernHigh-resolution mass spectrometryMulti-layered SPEPharmaceuticalsStreams

Identifiers

PMID36926270
PMCPMC10011426
OpenAlexW4321792609

What OpenQuestion holds

Textfull text, public
LicenceCC BY
reference markers read1
measurements read35
identifiers read1
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.