Evidence map›Paper›PMID 36849617›Full record

ArticleAnalytical and bioanalytical chemistry2023

Quantitation of guanidine derivatives as representative persistent and mobile organic compounds in water: method development.

Makiko Ichihara, Daichi Asakawa, Atsushi Yamamoto, Miki Sudo

Open access · hybridFull text read
In one paragraph

Article in Analytical and bioanalytical chemistry, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 4 papers.

0numbers the graph read from it
0cells of the map it votes in
4citing papers in PubMed
2.1field-weighted citation impact, top 15% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

4 citing papers in PubMed, 14 citations in OpenAlex.

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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

4 authors at 3 institutions in 1 country.

Makiko IchiharaOsaka City Research Center of Environmental Science, 1-3-3 Nakamichi, Higashinari-Ku, Osaka, 537-0025, Japan. mak-ichihara@city.osaka.lg.jp.ORCID http://orcid.org/0000-0002-5758-7741
Daichi AsakawaOsaka City Research Center of Environmental Science, 1-3-3 Nakamichi, Higashinari-Ku, Osaka, 537-0025, Japan.
Atsushi YamamotoFaculty of Environmental Studies, Tottori University of Environmental Studies, 1-1-1 Wakabadai-Kita, Tottori, Tottori, 689-1111, Japan.
Miki SudoDepartment of Biological Resources Management, School of Environmental Science, The University of Shiga Prefecture, 2500 Hassaka-Cho, Hikone, Shiga, 522-8533, Japan.
Osaka City University · JPTottori University of Environmental Studies · JPUniversity of Shiga Prefecture · JP

Funding

JSPS KAKENHI JP20K12214
6 · The paper itself

Abstract

Persistent and mobile organic compounds (PMOCs) are highly soluble in water, thereby posing a threat to water resource quality. Currently, there are no methods that can accurately quantify guanidine derivative PMOCs, other than 1,3-diphenylguanidine (DPG) and cyanoguanidine (CG), in aqueous media. In this study, we developed a quantitation method that combines solid-phase extraction and liquid chromatography (LC)-tandem mass spectrometry to detect seven guanidine derivatives in aquatic environments and applied it to environmental water samples. Five LC columns were examined, and among them, a hydrophilic interaction liquid chromatography column was chosen owing to its suitable instrument detection limit and retention factor. Method precision was assessed using seven replicate analyses of river water. The corresponding analyte recoveries ranged from 73 to 137% (coefficient of variation = 2.1-5.8%). DPG and CG were detected in ultrapure water samples at levels up to 0.69 and 150 ng L

Indexed as

1,3-DiphenylguanidineAnalytical method developmentCyanoguanidineGuanidine derivativeHydrophilic interaction liquid chromatography (HILIC)Persistent and mobile organic compounds (PMOCs)

Identifiers

PMID36849617
PMCPMC10050033
OpenAlexW4322487386

What OpenQuestion holds

Textfull text, public
LicenceCC BY
measurements read43
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.