Evidence map›Paper›PMID 36820909›Full record

ArticleAnalytical and bioanalytical chemistry2023

Liquid-phase microextraction of aromatic amines: hollow fiber-liquid-phase microextraction and parallel artificial liquid membrane extraction comparison.

Nerea Lorenzo-Parodi, Wiebke Kaziur-Cegla, Astrid Gjelstad, Torsten C Schmidt

Open access · hybridAbstract read
In one paragraph

Article in Analytical and bioanalytical chemistry, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 9 papers.

0numbers the graph read from it
0cells of the map it votes in
9citing papers in PubMed
3.0field-weighted citation impact, top 9% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

9 citing papers in PubMed, 22 citations in OpenAlex.

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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

4 authors at 3 institutions in 2 countries.

Nerea Lorenzo-ParodiInstrumental Analytical Chemistry, University of Duisburg-Essen, Universitätsstrasse 5, 45141, Essen, Germany.ORCID http://orcid.org/0000-0002-4761-5403
Wiebke Kaziur-CeglaInstrumental Analytical Chemistry, University of Duisburg-Essen, Universitätsstrasse 5, 45141, Essen, Germany.
Astrid GjelstadDepartment of Pharmacy, University of Oslo, Blindern, P.O. Box 1068, 0316, Oslo, Norway.ORCID http://orcid.org/0000-0002-4444-1794
Torsten C SchmidtInstrumental Analytical Chemistry, University of Duisburg-Essen, Universitätsstrasse 5, 45141, Essen, Germany. torsten.schmidt@uni-due.de.ORCID http://orcid.org/0000-0003-1107-4403
University of Duisburg-Essen · DEIWW Water Centre · DEUniversity of Oslo · NO

Funding

Evonik Industries PhD scholarship NLP
6 · The paper itself

Abstract

Aromatic amines (AA) are carcinogenic compounds that can enter the human body through many sources, one of the most important being tobacco smoke. They are excreted with the urine, from which they can be extracted and measured. To that end, hollow fiber-liquid-phase microextraction (HF-LPME) and parallel artificial liquid membrane extraction (PALME) were optimized for the analysis of representative aromatic amines, as alternatives to liquid-liquid extraction (LLE). Relevant extraction parameters, namely organic solvent, extraction time, agitation speed, and acceptor solution pH, were studied, and the two optimized techniques-HF-LPME: dihexyl ether, 45 min, 250 rpm, and pH 1; PALME: undecane, 20 min, 250 rpm and pH 1-were compared. Comparison of the optimized methods showed that significantly higher recoveries could be obtained with PALME than with HF-LPME. Therefore, PALME was further validated. The results were successful for nine different AA, with regression coefficients (R

Indexed as

Liquid Phase MicroextractionMembranes, ArtificialAminesHumansLiquid-Liquid ExtractionSolventsAminesMembranes, ArtificialSolventsAromatic aminesGC–MSHollow fiber-liquid-phase microextraction (HF-LPME)Liquid–liquid extractionParallel artificial liquid membrane extraction (PALME)Urine

Identifiers

PMID36820909
PMCPMC9992073
OpenAlexW4321599468

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.