Evidence map›Paper›PMID 36811757›Full record

ArticleAnalytical sciences : the international journal of the Japan Society for Analytical Chemistry2023

Solid-phase microextraction with MIL-53(Al)-polymer monolithic column coupled to pressurized capillary electrochromatography for determination of chlorogenic acid and ferulic acid in sugarcane samples.

Tingfan Tang, Xiaohui Li, Jiaqing Zhu, Wenyi Huang, Hao Cheng, Jun Feng

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Article in Analytical sciences : the international journal of the Japan Society for Analytical Chemistry, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

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Tingfan Tang *Guangxi Key Laboratory of Green Processing of Sugar Resources, School of Medicine, College of Biological and Chemical Engineering, Guangxi Zhuang Autonomous Region, Guangxi University of Science and Technology, No.257 Liushi Road, Yufeng District, Liuzhou, 545006, Guangxi, People's Republic of China.
Xiaohui Li *Guangxi Key Laboratory of Green Processing of Sugar Resources, School of Medicine, College of Biological and Chemical Engineering, Guangxi Zhuang Autonomous Region, Guangxi University of Science and Technology, No.257 Liushi Road, Yufeng District, Liuzhou, 545006, Guangxi, People's Republic of China.
Jiaqing ZhuGuangxi Key Laboratory of Green Processing of Sugar Resources, School of Medicine, College of Biological and Chemical Engineering, Guangxi Zhuang Autonomous Region, Guangxi University of Science and Technology, No.257 Liushi Road, Yufeng District, Liuzhou, 545006, Guangxi, People's Republic of China.
Wenyi HuangGuangxi Key Laboratory of Green Processing of Sugar Resources, School of Medicine, College of Biological and Chemical Engineering, Guangxi Zhuang Autonomous Region, Guangxi University of Science and Technology, No.257 Liushi Road, Yufeng District, Liuzhou, 545006, Guangxi, People's Republic of China.
Hao ChengGuangxi Key Laboratory of Green Processing of Sugar Resources, School of Medicine, College of Biological and Chemical Engineering, Guangxi Zhuang Autonomous Region, Guangxi University of Science and Technology, No.257 Liushi Road, Yufeng District, Liuzhou, 545006, Guangxi, People's Republic of China.
Jun FengGuangxi Key Laboratory of Green Processing of Sugar Resources, School of Medicine, College of Biological and Chemical Engineering, Guangxi Zhuang Autonomous Region, Guangxi University of Science and Technology, No.257 Liushi Road, Yufeng District, Liuzhou, 545006, Guangxi, People's Republic of China. hxpfengjun@gxust.edu.cn.ORCID http://orcid.org/0000-0003-0828-1575

Funding

Natural Science Foundation of Guangxi Province 2016GXNSFAA380108Natural Science Foundation of Guangxi Province 2019GXNSFDA245025Natural Science Foundation of Guangxi Province 2020GXNSFAA 297168State Key Laboratory for Chemistry and Molecular Engineering of Medicinal Resources CMEMR2019- B10
6 · The paper itself

Abstract

In this paper, a polymer monolithic column based on poly (Butyl methacrylate-co-ethylene glycol dimethacrylate) (poly (BMA-co-EDGMA)) doped with MIL-53(Al) metal-organic framework (MOF) was prepared using an in situ polymerization method. The characteristics of MIL-53(Al)-polymer monolithic column were studied through scanning electron microscopy (SEM), Fourier transform infrared spectrometry (FT-IR), energy-dispersive spectroscopy (EDS), X-ray powder diffractometry (XRD), and nitrogen adsorption experiment. Due to its large surface area, the prepared MIL-53(Al)-polymer monolithic column has good permeability and high extraction efficiency. Using MIL-53(Al)-polymer monolithic column for solid-phase microextraction (SPME), coupled to pressurized capillary electrochromatography (pCEC), a method for the determination of trace chlorogenic acid and ferulic acid in sugarcane was established. Under optimized conditions, chlorogenic acid and ferulic acid have a good linear relationship (r ≥ 0.9965) within the concentration range of 50.0-500 µg/mL, the detection limit is 0.017 µg/mL, and the relative standard deviation (RSD) is less than 3.2%. The spike recoveries of chlorogenic acid and ferulic acid were 96.5% and 96.7%, respectively. The results indicate that the method is sensitive, practical, and convenient. It has been successfully applied to the separation and detection of trace organic phenolic compounds in sugarcane samples.

Indexed as

Capillary ElectrochromatographySaccharumChlorogenic AcidCoumaric AcidsPolymersSolid Phase MicroextractionSpectroscopy, Fourier Transform InfraredChlorogenic AcidCoumaric Acidsferulic acidPolymersMetal–organic framework (MOF)Monolithic columnOrganic phenolic acid compoundsPressurized capillary electrochromatography (pCEC)Solid-phase microextraction (SPME)Sugarcane

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PMID36811757

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