Evidence map›Paper›PMID 36777141›Full record

ArticleJournal of applied crystallography2023

Extracting the morphology of gold bipyramids from small-angle X-ray scattering experiments via form factor modelling.

Jieli Lyu, Claire Goldmann, Cyrille Hamon, Doru Constantin

Abstract read
In one paragraph

Article in Journal of applied crystallography, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Article
  2. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

4 authors.

Jieli LyuLaboratoire de Physique des Solides, CNRS, Université Paris-Sud, Université Paris-Saclay, 91405 Orsay Cedex, France.ORCID https://orcid.org/0000-0003-1549-8975
Claire GoldmannLaboratoire de Physique des Solides, CNRS, Université Paris-Sud, Université Paris-Saclay, 91405 Orsay Cedex, France.
Cyrille HamonLaboratoire de Physique des Solides, CNRS, Université Paris-Sud, Université Paris-Saclay, 91405 Orsay Cedex, France.
Doru ConstantinInstitut Charles Sadron, CNRS and Université de Strasbourg, 67034 Strasbourg, France.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Accurate shape description is a challenge in materials science. Small-angle X-ray scattering (SAXS) can provide the shape, size and polydispersity of nanoparticles by form factor modelling. However, simple geometric models such as the ellipsoid may not be enough to describe objects with complex shapes. This work shows that the form factor of gold nanobipyramids is accurately described by a truncated bicone model, which is validated by comparison with transmission electron microscopy (TEM) data for nine different synthesis batches; the average shape parameters (width, height and truncation) and the sample polydispersity are obtained. In contrast, the ellipsoid model yields worse fits of the SAXS data and exhibits systematic discrepancies with the TEM results.

Indexed as

bipyramidscolloidsform factorsSAXSsmall-angle X-ray scatteringTEMtransmission electron microscopy

Identifiers

PMID36777141
PMCPMC9901920

What OpenQuestion holds

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.