ArticleACS applied materials & interfaces2023
Nano-FTIR Spectroscopy of the Solid Electrolyte Interphase Layer on a Thin-Film Silicon Li-Ion Anode.
Article in ACS applied materials & interfaces, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 11 papers.
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Who cites it
11 citing papers in PubMed.
- Heat Transfer Fluids as Co-Diluents in Localized High-Concentration Electrolytes for High-Rate Lithium Metal Batteries With Enhanced Safety.Angewandte Chemie (International ed. in English) · 2026Article
- Efficient Non-Invasive Rejuvenation of Spent Lithium Iron Phosphate Batteries Through Controlled Overdischarge.Advanced materials (Deerfield Beach, Fla.) · 2026Article
- A Quaternary Ammonium-Modified Resin for Selective Perchlorate Removal from Fireworks Wastewater.Polymers · 2026Article
- Structural Evolution of Silicon Nitride Anodes during Electrochemical Lithiation.ACS electrochemistry · 2025Article
- An infrared, Raman, and X-ray database of battery interphase components.Scientific data · 2025Article
- Long term porosity of solid electrolyte interphase on model silicon anodes with liquid battery electrolytes.Communications chemistry · 2024Article
- Article
- Promoting Homogeneous Zinc-Ion Transfer Through Preferential Ion Coordination Effect in Gel Electrolyte for Stable Zinc Metal Batteries.Advanced science (Weinheim, Baden-Wurttemberg, Germany) · 2023Article
- Article
- FTIR spectrum analysis to predict the crystalline and amorphous phases of hydroxyapatite: a comparison of vibrational motion to reflection.RSC advances · 2023Article
- Article
Corrections and comments
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Authors and funding
5 authors.
Funding
No grant is acknowledged in the PubMed record.
Abstract
Si anodes for Li-ion batteries are notorious for their large volume expansion during lithiation and the corresponding detrimental effects on cycle life. However, calendar life is the primary roadblock for widespread adoption. During calendar life aging, the main origin of impedance increase and capacity fade is attributed to the instability of the solid electrolyte interphase (SEI). In this work, we use ex situ nano-Fourier transform infrared spectroscopy and X-ray photoelectron spectroscopy to characterize the structure and composition of the SEI layer on amorphous Si thin films after an accelerated calendar aging protocol. The characterization of the SEI on non-washed and washed electrodes shows that brief washing in dimethyl carbonate results in large changes to the film chemistry and topography. Detailed examination of the non-washed electrodes during the first lithiation and after an accelerated calendar aging protocol reveals that PF
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