Evidence map›Paper›PMID 36676223›Full record

ArticleMaterials (Basel, Switzerland)2023

Electron Beam Irradiation on the Production of a Si- and Zr-Based Hybrid Material: A Study by FTIR and WDXRF.

Alexandra P Rodrigues, Pedro M P Santos, João Pedro Veiga, Maria Helena Casimiro, Luís M Ferreira

Abstract read
In one paragraph

Article in Materials (Basel, Switzerland), 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed.

  1. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

5 authors.

Alexandra P RodriguesCentro de Ciências e Tecnologias Nucleares (C2TN), Instituto Superior Técnico, Universidade de Lisboa, Estrada Nacional 10, km 139,7, Bobadela, 2695-066 Loures, Portugal.ORCID 0000-0001-6300-3880
Pedro M P SantosCentro de Ciências e Tecnologias Nucleares (C2TN), Instituto Superior Técnico, Universidade de Lisboa, Estrada Nacional 10, km 139,7, Bobadela, 2695-066 Loures, Portugal.ORCID 0000-0002-3363-0098
João Pedro VeigaDepartamento de Conservação e Restauro (DCR), Faculdade de Ciências e Tecnologia, Universidade NOVA de Lisboa, Campus de Caparica, 2829-516 Caparica, Portugal.ORCID 0000-0001-5324-1586
Maria Helena CasimiroCentro de Ciências e Tecnologias Nucleares (C2TN), Instituto Superior Técnico, Universidade de Lisboa, Estrada Nacional 10, km 139,7, Bobadela, 2695-066 Loures, Portugal.ORCID 0000-0003-0893-0686
Luís M FerreiraCentro de Ciências e Tecnologias Nucleares (C2TN), Instituto Superior Técnico, Universidade de Lisboa, Estrada Nacional 10, km 139,7, Bobadela, 2695-066 Loures, Portugal.

Funding

Fundação para a Ciência e Tecnologia PD/BD/114410/2016Fundação para a Ciência e Tecnologia UIDB/04349/2020Fundação para a Ciência e Tecnologia UIDB/50025/2020-2023International Atomic Energy Agency 18982 of CRP F23032International Atomic Energy Agency 23186 of CRP F22070
6 · The paper itself

Abstract

Sol-gel production of hybrid materials has, to some extent, revolutionised materials' engineering and the way science and technology perceive the creation of new materials. Despite that, the method presents some limitations that are circumvented by radiation processing. Electron beam irradiation was used to promote synthesis of hybrid structures while using silanol-terminated PDMS, TEOS and TPOZ as precursors. Evaluation of the method's performance was executed by gel fraction determination, WDXRF and FTIR-ATR. Results showed that, although there is some pre-irradiation reactivity between precursors, radiolysis induces scission on multiple sites of precursor's structures, which induces hybrid network formation to a greater extent. Characterisation allowed determining electron beam irradiation to be effective in the creation of Si-O-Zr bonds, resulting in the production of a Class II hybrid material.

Indexed as

electron beamhybrid materialsPDMSradiation processingTEOSzirconium

Identifiers

PMID36676223
PMCPMC9862691

What OpenQuestion holds

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.