ArticleMolecules (Basel, Switzerland)2023
Advanced Fitting Method for the Kinetic Analysis of Thermogravimetric Data.
Article in Molecules (Basel, Switzerland), 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 3 papers.
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3 citing papers in PubMed.
- Effect of Olive Stone Biomass Ash Filler in Polylactic Acid Biocomposites on Accelerated Weathering Tests.Polymers · 2025Article
- Thermogravimetric analysis and kinetic modeling of the pyrolysis of different biomass types by means of model-fitting, model-free and network modeling approaches.Journal of thermal analysis and calorimetry · 2024Article
- Thermal Degradation Studies of Poly(2-ethyl hexyl acrylate) in the Presence of Nematic Liquid Crystals.Polymers · 2023Article
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4 authors.
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Abstract
The article considered the solution of the inverse problem of chemical kinetics of the analysis of experimental data of a thermogravimetric experiment at a constant sample heating rate. The fitting method for identifying the parameters of a kinetic triplet using the integral method for a model of a solid-state reaction based on the modified Arrhenius equation is described. The effectiveness of the proposed approach was confirmed by solving test cases for low, medium, and high rates of material conversion. Unlike other methods, setting the parameters of the reaction mechanism is not required, as they are determined by the solution. Solutions for real data of TGA studies with high and low sample heating rates were compared with the results obtained by other authors and experimental data. A description of the full cycle of calculations used to identify kinetic parameters from thermogravimetric experimental data is given, from the derivation of calculated relationships to the implementation of a short (three to five formulas) program code for MS Excel spreadsheets. The presented code is easy to verify and reproduce and can be modified to solve various problems.
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