Evidence map›Paper›PMID 36595940›Full record

ArticleSTAR protocols2022

Protocol for microwave-assisted synthesis of unsymmetrical azo dyes.

Ankit Thakuri, Mainak Banerjee, Amrita Chatterjee

Abstract read
In one paragraph

Article in STAR protocols, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

0numbers the graph read from it
0cells of the map it votes in
0citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

0 citing papers in PubMed.

No citing paper in PubMed yet.

4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

3 authors.

Ankit ThakuriDepartment of Chemistry, BITS-Pilani, K.K. Birla Goa Campus, NH 17B, Bypass Road, Zuarinagar, Sancoale, Goa 403726, India.
Mainak BanerjeeDepartment of Chemistry, BITS-Pilani, K.K. Birla Goa Campus, NH 17B, Bypass Road, Zuarinagar, Sancoale, Goa 403726, India. Electronic address: mainak@goa.bits-pilani.ac.in.
Amrita ChatterjeeDepartment of Chemistry, BITS-Pilani, K.K. Birla Goa Campus, NH 17B, Bypass Road, Zuarinagar, Sancoale, Goa 403726, India. Electronic address: amrita@goa.bits-pilani.ac.in.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Aromatic azo dyes bear immense commercial significance because of their extensive usage in the textile, paint, and food industries. With growing environmental concerns, developing alternative greener approaches for the synthesis of azo dyes is crucial. Herein, we describe a metal-free, microwave (MW)-assisted protocol for rapid access to a large variety of unsymmetrical azo dyes by coupling nitroarenes and aromatic amines. After MW-assisted coupling, the azo dyes are then isolated by precipitation followed by recrystallization to obtain pure azo dyes. For complete details on the use and execution of this protocol, please refer to Thakuri et al. (2022).

Indexed as

Azo CompoundsMicrowavesAminesTextilesAminesAzo CompoundsChemistryEnvironmental sciences

Identifiers

PMID36595940
PMCPMC9678771

What OpenQuestion holds

Textmetadata
LicenceCC BY-NC-ND
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.