ArticleJournal of applied crystallography2022
Improving data quality for three-dimensional electron diffraction by a post-column energy filter and a new crystal tracking method.
Article in Journal of applied crystallography, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 12 papers.
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Who cites it
12 citing papers in PubMed.
- Characterization of energy filtering slit widths for MicroED data collection.Journal of structural biology: X · 2026Article
- Electrons and X-rays for diffraction and imaging.Acta crystallographica. Section D, Structural biology · 2026Review
- Direct from the seed: an atomic resolution protein structure by ab initio MicroED.Nature communications · 2026Article
- 3D Electron Diffraction on Nanoparticles: Minimal Size and Associated Dynamical Effects.ACS nano · 2025Article
- Recovering high-resolution information using energy filtering in MicroED.Structural dynamics (Melville, N.Y.) · 2025Article
- Polymorphism in oxyresveratrol studied by 3D ED.ACS omega · 2024Article
- The crystal structure of olanzapine form III.IUCrJ · 2024Article
- Reaching the potential of electron diffraction.Cell reports. Physical science · 2024Article
- Parameterized absorptive electron scattering factors.Acta crystallographica. Section A, Foundations and advances · 2024Article
- Modelling dynamical 3D electron diffraction intensities. II. The role of inelastic scattering.Acta crystallographica. Section A, Foundations and advances · 2024Article
- Electron crystallography and dedicated electron-diffraction instrumentation.Acta crystallographica. Section E, Crystallographic communications · 2023Article
- Electron Diffraction of 3D Molecular Crystals.Chemical reviews · 2022Review
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3 authors.
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Abstract
Three-dimensional electron diffraction (3D ED) has become an effective technique to determine the structures of submicrometre- (nanometre-)sized crystals. In this work, energy-filtered 3D ED was implemented using a post-column energy filter in both STEM mode and TEM mode [(S)TEM denoting (scanning) transmission electron microscope]. The setups for performing energy-filtered 3D ED on a Gatan imaging filter are described. The technique and protocol improve the accessibility of energy-filtered 3D ED post-column energy filters, which are available in many TEM laboratories. In addition, a crystal tracking method in STEM mode using high-angle annular dark-field imaging is proposed. This method enables the user to monitor the crystal position while collecting 3D ED data at the same time, allowing a larger tilt range without foregoing any diffraction frames or imposing extra electron dose. In order to compare the differences between energy-filtered and unfiltered 3D ED data sets, three well known crystallized inorganic samples have been studied in detail. For these samples, the final
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