Evidence map›Paper›PMID 36530536›Full record

ArticleBeilstein journal of organic chemistry2022

A novel bis-triazole scaffold accessed via two tandem [3 + 2] cycloaddition events including an uncatalyzed, room temperature azide-alkyne click reaction.

Ksenia Malkova, Andrey Bubyrev, Vasilisa Krivovicheva, Dmitry Dar'in, Alexander Bunev, Mikhail Krasavin

Abstract read
In one paragraph

Article in Beilstein journal of organic chemistry, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

0numbers the graph read from it
0cells of the map it votes in
0citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

0 citing papers in PubMed.

No citing paper in PubMed yet.

4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors.

Ksenia MalkovaSaint Petersburg State University, Saint Petersburg 199034, Russian Federation.
Andrey BubyrevSaint Petersburg State University, Saint Petersburg 199034, Russian Federation.
Vasilisa KrivovichevaSaint Petersburg State University, Saint Petersburg 199034, Russian Federation.
Dmitry Dar'inSaint Petersburg State University, Saint Petersburg 199034, Russian Federation.ORCID https://orcid.org/0000-0002-0413-7413
Alexander BunevMedicinal Chemistry Center, Togliatti State University,445020 Togliatti, Russian Federation.ORCID https://orcid.org/0000-0001-6408-8329
Mikhail KrasavinSaint Petersburg State University, Saint Petersburg 199034, Russian Federation.ORCID https://orcid.org/0000-0002-0200-4772

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

The previously described α-acetyl-α-diazomethanesulfonamide was employed in a three-component reaction with azide-containing benzaldehydes and propargylamines. Besides the initial formation of the triazole core, the reaction proceeded further, in uncatalyzed fashion at room temperature and yielded, after intramolecular azide-alkyne click reaction novel, structurally intriguing bistriazoles.

Indexed as

1,2,3-triazolesintramolecular click reactionroom temperatureuncatalyzedα-acetyl-α-diazomethane sulfonamide

Identifiers

PMID36530536
PMCPMC9727270

What OpenQuestion holds

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.