ArticleToxicology reports2023
Simultaneous determination of antibiotics residues in edible fish muscle using eco-friendly SPE-UPLC-MS/MS: Occurrence, human dietary exposure and health risk assessment for consumer safety.
Article in Toxicology reports, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 14 papers.
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Who cites it
14 citing papers in PubMed, 34 citations in OpenAlex.
- Zein-templated synthesis of Au@Pt bimetallic nanozymes: a multi-mode lateral flow immunoassay platform for ultrasensitive colorimetric and fluorometric detection of tetracycline in food.Mikrochimica acta · 2026Article
- A Systematic Review of On-Site Rapid Detection Methods for Antibiotic Residues in Aquatic Products (2021-2025).Foods (Basel, Switzerland) · 2026Review
- HPLC and CE Procedures for the Determination of Fluoroquinolones (2020-2025).Molecules (Basel, Switzerland) · 2026Review
- Sustainable Anisaldehyde-Based Natural Deep Eutectic Solvent Dispersive Liquid-Liquid Microextraction for Monitoring Antibiotic Residues in Commercial Milk and Eggs: A Comprehensive Evaluation of Greenness, Practicality, Analytical Performance and Innovation.Foods (Basel, Switzerland) · 2026Article
- Optimization of SERS Detection for Sulfathiazole Residues in Chicken Blood Using GA-SVR.Foods (Basel, Switzerland) · 2026Article
- Development and Validation of QuEChERS Extraction Coupled with Ultrahigh-Performance Liquid Chromatography-Tandem Mass Spectrometry for the Detection of Nine Macrolides in Fish Products.Foods (Basel, Switzerland) · 2025Article
- High prevalence of low-concentration antimicrobial residues in commercial fish: A public health concern in Bangladesh.PloS one · 2025Article
- Insights into the sustainability of liquid chromatographic methods for favipiravir bioanalysis: a comparative study.RSC advances · 2024Review
- Article
- Bioaccumulation of Organic and Inorganic Pollutants in Fish from Thermaikos Gulf: Preliminary Human Health Risk Assessment Assisted by a Computational Approach.Journal of xenobiotics · 2024Article
- Determination of Multiclass Antibiotics in Fish Muscle Using a QuEChERS-UHPLC-MS/MS Method.Foods (Basel, Switzerland) · 2024Article
- Article
- Dispersive Solid-Phase Extraction and Ultra-Performance Liquid Chromatography-Tandem Mass Spectrometry-A Rapid and Accurate Method for Detecting 10 Macrolide Residues in Aquatic Products.Foods (Basel, Switzerland) · 2024Article
- Health Risk Assessment of Antibiotic Pollutants in Large Yellow Croakers from Zhejiang Aquaculture Sites.Foods (Basel, Switzerland) · 2023Article
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Authors and funding
2 authors at 1 institution in 1 country.
Funding
No grant is acknowledged in the PubMed record.
Abstract
Occurrence of multi-class antibiotics in edible fish species from the Saudi market was investigated. A fast and sensitive UPLC-MS/MS method for simultaneous determination of selected fluoroquinolones, sulfonamides and macrolides in fish muscle was developed and validated. Sample clean up was performed using solid-phase extraction on Oasis HLB cartridges. The greenness profile of the developed method was evaluated using three assessment tools: analytical Eco-scale assessment method, green analytical procedure index and analytical greenness metric. Detection limits ranged from 0.008 to 0.35 μg/kg. The recovery ranged from 80.1 % to 98.6 % with RSDs ≤ 12.1 %. The mean and maximum concentrations of the detected antibiotics in fish samples ranged between 0.28 and 19.15 and 3.50-112.00 µg/kg, respectively. Human antibiotics (clarithromycin and roxithromycin) were detected in 50 % and 27.5 % of the samples, respectively. The estimated daily intake for the detected antibiotics ranged from 0.10 to 6.61 ng/kg/ BW/day for Saudi adults. The health risk associated with fish consumption was evaluated. The results suggested that fish consumption may not pose a serious risk to consumers in Saudi Arabia. The developed method was fast, sensitive, cost-effective and environmentally friendly.
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