ArticleJACS Au2022
Solid-State NMR Spectra of Protons and Quadrupolar Nuclei at 28.2 T: Resolving Signatures of Surface Sites with Fast Magic Angle Spinning.
Article in JACS Au, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 6 papers.
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Who cites it
6 citing papers in PubMed.
- Article
- 40 Tesla miniature magnets.Science advances · 2026Article
- Review
- Solid-State Nuclear Magnetic Resonance Spectroscopy for Surface Characterization of Metal Oxide Nanoparticles: State of the Art and Perspectives.Journal of the American Chemical Society · 2025Review
- Nuclear spin polarization of lactic acid via exchange of parahydrogen-polarized protons.Communications chemistry · 2024Article
- Tailored Lewis Acid Sites for High-Temperature Supported Single-Molecule Magnetism.Journal of the American Chemical Society · 2023Article
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Authors and funding
7 authors.
Funding
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Abstract
Advances in solid-state nuclear magnetic resonance (NMR) methods and hardware offer expanding opportunities for analysis of materials, interfaces, and surfaces. Here, we demonstrate the application of a very high magnetic field strength of 28.2 T and fast magic-angle-spinning rates (MAS, >40 kHz) to surface species relevant to catalysis. Specifically, we present as case studies the 1D and 2D solid-state NMR spectra of important catalyst and support materials, ranging from a well-defined silica-supported organometallic catalyst to dehydroxylated γ-alumina and zeolite solid acids. The high field and fast-MAS measurement conditions substantially improve spectral resolution and narrow NMR signals, which is particularly beneficial for solid-state 1D and 2D NMR analysis of
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