Evidence map›Paper›PMID 36431882›Full record

ArticleMolecules (Basel, Switzerland)2022

High-Pressure Supercritical CO

Lacrimioara Senila, Daniela Alexandra Scurtu, Eniko Kovacs, Erika Andrea Levei, Oana Cadar, Anca Becze, Cerasel Varaticeanu

Abstract read
In one paragraph

Article in Molecules (Basel, Switzerland), 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Article
  2. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

7 authors.

Lacrimioara SenilaResearch Institute for Analytical Instrumentation Subsidiary, National Institute for Research and Development for Optoelectronics Bucharest INOE 2000, 67 Donath Street, 400293 Cluj-Napoca, Romania.ORCID 0000-0002-5791-0449
Daniela Alexandra ScurtuResearch Institute for Analytical Instrumentation Subsidiary, National Institute for Research and Development for Optoelectronics Bucharest INOE 2000, 67 Donath Street, 400293 Cluj-Napoca, Romania.ORCID 0000-0002-5941-1213
Eniko KovacsResearch Institute for Analytical Instrumentation Subsidiary, National Institute for Research and Development for Optoelectronics Bucharest INOE 2000, 67 Donath Street, 400293 Cluj-Napoca, Romania.ORCID 0000-0003-1970-0923
Erika Andrea LeveiResearch Institute for Analytical Instrumentation Subsidiary, National Institute for Research and Development for Optoelectronics Bucharest INOE 2000, 67 Donath Street, 400293 Cluj-Napoca, Romania.ORCID 0000-0002-0145-0287
Oana CadarResearch Institute for Analytical Instrumentation Subsidiary, National Institute for Research and Development for Optoelectronics Bucharest INOE 2000, 67 Donath Street, 400293 Cluj-Napoca, Romania.ORCID 0000-0002-0879-9211
Anca BeczeResearch Institute for Analytical Instrumentation Subsidiary, National Institute for Research and Development for Optoelectronics Bucharest INOE 2000, 67 Donath Street, 400293 Cluj-Napoca, Romania.ORCID 0000-0003-1418-689X
Cerasel VaraticeanuResearch Institute for Analytical Instrumentation Subsidiary, National Institute for Research and Development for Optoelectronics Bucharest INOE 2000, 67 Donath Street, 400293 Cluj-Napoca, Romania.

Funding

Ministry of Research, Technology and Higher Education Ministry of Research, Innovation and Digitization, CNCNS-UEFISCDI, project number PN-III-P1.1.1-TE-2021-0179, within PNCDI III, LIGNOBIOPLAST.
6 · The paper itself

Abstract

This study's objective was to separate cellulose, hemicellulose, and lignin after high-pressure supercritical carbon dioxide pretreatment for further valorization. The study investigated the supercritical carbon dioxide pretreatment of apple orchard waste at temperatures of 160-200 °C, for 15-45 min, at a pressure of 10 MPa. Response Surface Methodology (RSM) was used to optimize the supercritical process and to improve its efficiency. The change of functional groups during different pretreatment conditions was examined by Fourier transform infrared (FTIR) spectroscopy. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) confirmed the structural changes in the biomass structure before and after pretreatment. A new ultra-high performance liquid chromatography (UHPLC) coupled with an evaporative light scattering detector (ELSD) method was developed and validated for the determination of carbohydrates in the liquid fraction that resulted after pretreatment. The estimated uncertainty of the method ranged from 16.9 to 20.8%. The pre-treatment of high-pressure supercritical CO

Indexed as

Carbon DioxideMalusCarbohydratesHexosesLigninUncertaintyCarbohydratesCarbon DioxideHexosesLigninapple orchard wasteRSMsupercritical carbon dioxide pretreatmentUHPLCvalidation

Identifiers

PMID36431882
PMCPMC9692898

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.