ArticleFoods (Basel, Switzerland)2022
Validation of a Multi-Residue Analysis Method for 287 Pesticides in Citrus Fruits Mandarin Orange and Grapefruit Using Liquid Chromatography-Tandem Mass Spectrometry.
Article in Foods (Basel, Switzerland), 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 10 papers.
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Who cites it
10 citing papers in PubMed, 25 citations in OpenAlex.
- Acidified Acetonitrile Extraction and Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry for Multiresidue Determination of 136 Pesticides in Tahiti Lime (Foods (Basel, Switzerland) · 2026Article
- Citrus Essential Oils: A Review of Chemical Composition, Bioactivity, Safe Use, and Potential Applications.Chemistry & biodiversity · 2026Review
- The Impact of High Urban Temperatures on Pesticide Residues Accumulation in Vegetables Grown in the Greater Accra Metropolitan Area of Ghana.Journal of xenobiotics · 2025Article
- Levels of organochlorine pesticides in onion and tomato samples from selected towns of Jimma Zone, Ethiopia.Heliyon · 2024Article
- Article
- Simultaneous Screening of 322 Residual Pesticides in Fruits and Vegetables Using GC-MS/MS and Deterministic Health Risk Assessments.Foods (Basel, Switzerland) · 2023Article
- Factors Affecting Incurred Pesticide Extraction in Cereals.Molecules (Basel, Switzerland) · 2023Article
- Multivariate Assessment and Risk Ranking of Pesticide Residues in Citrus Fruits.Foods (Basel, Switzerland) · 2023Article
- Low-Temperature Cleanup Followed by Dispersive Solid-Phase Extraction for Determination of Nine Polar Plant Growth Regulators in Herbal Matrices Using Liquid Chromatography-Tandem Mass Spectrometry.Chromatographia · 2023Article
- A review on recent advances in mass spectrometry analysis of harmful contaminants in food.Frontiers in nutrition · 2023Review
Corrections and comments
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Authors and funding
10 authors at 2 institutions in 1 country.
Funding
Abstract
Since the introduction of the positive list system (PLS) for agricultural products in the Republic of Korea, the demand for a quick, easy multi-residue analysis method increased continuously. Herein, the quick, easy, cheap, effective, rugged, and safe (QuEChERS) technique combined with liquid chromatography−tandem mass spectrometry was employed to optimize a method for the multi-residue analysis of 287 pesticide residues in mandarin orange and grapefruit. Method validation was conducted in terms of selectivity, limit of quantitation (LOQ), linearity, accuracy, precision, and matrix effect. All the compounds at low spiking levels (1, 2.5, 5, or 10 mg/kg) could be quantified at LOQs lower than 0.01 mg/kg (PLS level). The linearity of the matrix-matched calibration curve for each compound is in the range 0.5−50 μg/L, and its coefficient of determination (R2) is >0.990. Satisfactory recovery values of 70−120% with a relative standard deviation of ≤20% are obtained for all compounds in the mandarin orange and grapefruit samples. A negligible matrix effect (−20−20%) is observed for more than 94.8% and 85.4% of the pesticides in mandarin orange and grapefruit, respectively. Therefore, this analytical method can contribute to pesticide residue analyses of citrus fruits for routine laboratory testing.
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