ArticleChemical science2022
Continuous-flow self-supported seATRP using a sonicated microreactor.
Article in Chemical science, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 3 papers.
What it found
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The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.
The trial behind it
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Who cites it
3 citing papers in PubMed.
- Scaling Organic Electrosynthesis: The Crucial Interplay between Mechanism and Mass Transport.ACS central science · 2025Article
- Simple Iron Halides Enable Electrochemically Mediated ATRP in Nonpolar Media.ACS macro letters · 2023Article
- Process intensification of continuous-flow seATRP by a sonicated multi-reactor setup.Reaction chemistry & engineering · 2023Article
Corrections and comments
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Authors and funding
3 authors.
Funding
No grant is acknowledged in the PubMed record.
Abstract
Continuous-flow simplified electrochemically mediated atom transfer radical polymerization (seATRP) was achieved for the first time without supporting electrolytes (self-supported) using a novel sonicated tubular microreactor. Polymerizations of different acrylic monomers were carried out under different applied currents. The reaction was fast with 75% conversion achieved at ambient temperature in less than 27 minutes. Results also showed good evolution of molecular weight and maintained narrow molecular weight distribution. The reaction rate can be further manipulated by tuning the applied current. Sonication under proper conditions was found to be able to significantly improve both reaction rate and controllability. Self-supported reactions also enable more environmentally friendly and cost-effective operations.
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Registered trials
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