ArticleJournal of synchrotron radiation2022
X-ray diffraction with micrometre spatial resolution for highly absorbing samples.
Article in Journal of synchrotron radiation, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 4 papers.
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Who cites it
4 citing papers in PubMed.
- Application of Synchrotron Radiation Based X-Ray Diffraction in Zeolite Research: Advanced Analysis from Atomic Structure to Dynamic Behavior.Advanced science (Weinheim, Baden-Wurttemberg, Germany) · 2025Review
- Multi-modal strain mapping of steel crack tips with micrometre spatial resolution.Journal of synchrotron radiation · 2025Article
- Quantitative Control of Oxygen Non-Stoichiometry and Negative Raman Chemical Shift During Topotactic Phase Transition in a Ca-Doped BiFeOAdvanced science (Weinheim, Baden-Wurttemberg, Germany) · 2025Article
- Ultimate sensitivity in X-ray diffraction: angular moments versus shot noise.Journal of applied crystallography · 2025Article
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Authors and funding
13 authors.
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Abstract
X-ray diffraction with high spatial resolution is commonly used to characterize (poly)crystalline samples with, for example, respect to local strain, residual stress, grain boundaries and texture. However, the investigation of highly absorbing samples or the simultaneous assessment of high-Z materials by X-ray fluorescence have been limited due to the utilization of low photon energies. Here, a goniometer-based setup implemented at the P06 beamline of PETRA III that allows for micrometre spatial resolution with a photon energy of 35 keV and above is reported. A highly focused beam was achieved by using compound refractive lenses, and high-precision sample manipulation was enabled by a goniometer that allows up to 5D scans (three rotations and two translations). As experimental examples, the determination of local strain variations in martensitic steel samples with micrometre spatial resolution, as well as the simultaneous elemental distribution for high-Z materials in a thin-film solar cell, are demonstrated. The proposed approach allows users from the materials-science community to determine micro-structural properties even in highly absorbing samples.
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