Evidence map›Paper›PMID 36320520›Full record

ArticleRSC advances2022

UiO-66-based metal-organic framework for dispersive solid-phase extraction of vanillylmandelic acid from urine before analysis by capillary electrophoresis.

Roghayeh Hassanpour-Sabet, Behruoz Seyfinejad, Elnaz Marzi Khosrowshahi, Mahboob Nemati, Mohammad Reza Afshar Mogaddam, Abolghasem Jouyban

Abstract read
In one paragraph

Article in RSC advances, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed.

  1. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors.

Roghayeh Hassanpour-SabetFood and Drug Safety Research Center, Tabriz University of Medical Sciences Tabriz Iran mr.afsharmogaddam@yahoo.com afsharmogaddam@tbzmed.ac.ir +98 41 31773333 +98 41 33372250.
Behruoz SeyfinejadPharmaceutical Analysis Research Center and Faculty of Pharmacy, Tabriz University of Medical Sciences Tabriz Iran ajouyban@hotmail.com.
Elnaz Marzi KhosrowshahiFood and Drug Safety Research Center, Tabriz University of Medical Sciences Tabriz Iran mr.afsharmogaddam@yahoo.com afsharmogaddam@tbzmed.ac.ir +98 41 31773333 +98 41 33372250.ORCID https://orcid.org/0000-0001-5502-9749
Mahboob NematiFood and Drug Safety Research Center, Tabriz University of Medical Sciences Tabriz Iran mr.afsharmogaddam@yahoo.com afsharmogaddam@tbzmed.ac.ir +98 41 31773333 +98 41 33372250.ORCID https://orcid.org/0000-0003-0458-0025
Mohammad Reza Afshar MogaddamFood and Drug Safety Research Center, Tabriz University of Medical Sciences Tabriz Iran mr.afsharmogaddam@yahoo.com afsharmogaddam@tbzmed.ac.ir +98 41 31773333 +98 41 33372250.ORCID https://orcid.org/0000-0003-1144-4523
Abolghasem JouybanPharmaceutical Analysis Research Center and Faculty of Pharmacy, Tabriz University of Medical Sciences Tabriz Iran ajouyban@hotmail.com.ORCID https://orcid.org/0000-0002-4670-2783

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Dispersive solid-phase extraction (DSPE) was developed for the extraction of vanillylmandelic acid (VMA) in urine samples prior to capillary electrophoresis with diode array detection (CE-DAD). Extraction of VMA by DSPE was carried out by direct addition of 7.5 mg of synthesized amino-functionalized UiO-66 (Zr) metal-organic framework adsorbent into the 5 mL sample solution (pH 4.0), followed by sonication and centrifugation. The supernatant layer was discarded, then the sedimented adsorbent was eluted using borate buffer (75 mM, pH 10). Effective extraction parameters including the amount of adsorbent, sample pH, adsorption and desorption time, type, volume and pH of eluent, and type of adsorbent dispersion method were systematically investigated. Under the optimized conditions, linearity of the method was from 40 to 2000 μg L

Identifiers

PMID36320520
PMCPMC9549476

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.