Evidence map›Paper›PMID 36296863›Full record

ArticleNanomaterials (Basel, Switzerland)2022

Synthesis and Optimization of Superhydrophilic-Superoleophobic Chitosan-Silica/HNT Nanocomposite Coating for Oil-Water Separation Using Response Surface Methodology.

Syarifah Nazirah Wan Ikhsan, Norhaniza Yusof, Farhana Aziz, Ahmad Fauzi Ismail, Norazanita Shamsuddin, Juhana Jaafar, Wan Norharyati Wan Salleh, Pei Sean Goh, Woei Jye Lau, Nurasyikin Misdan

Open access · goldAbstract read
In one paragraph

Article in Nanomaterials (Basel, Switzerland), 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
1.3field-weighted citation impact, top 23% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed, 17 citations in OpenAlex.

  1. Article
  2. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

10 authors at 3 institutions in 2 countries.

Syarifah Nazirah Wan IkhsanAdvanced Membrane Technology Research Centre (AMTEC), Block N29a, Universiti Teknologi Malaysia, Skudai 81310, Johor, Malaysia.
Norhaniza YusofAdvanced Membrane Technology Research Centre (AMTEC), Block N29a, Universiti Teknologi Malaysia, Skudai 81310, Johor, Malaysia.ORCID 0000-0003-1136-6246
Farhana AzizAdvanced Membrane Technology Research Centre (AMTEC), Block N29a, Universiti Teknologi Malaysia, Skudai 81310, Johor, Malaysia.
Ahmad Fauzi IsmailAdvanced Membrane Technology Research Centre (AMTEC), Block N29a, Universiti Teknologi Malaysia, Skudai 81310, Johor, Malaysia.
Norazanita ShamsuddinFaculty of Integrated Technologies, Universiti Brunei Darussalam, Bandar Seri Begawan BE1410, Brunei.ORCID 0000-0002-2281-502X
Juhana JaafarAdvanced Membrane Technology Research Centre (AMTEC), Block N29a, Universiti Teknologi Malaysia, Skudai 81310, Johor, Malaysia.
Wan Norharyati Wan SallehAdvanced Membrane Technology Research Centre (AMTEC), Block N29a, Universiti Teknologi Malaysia, Skudai 81310, Johor, Malaysia.ORCID 0000-0002-8212-3893
Pei Sean GohAdvanced Membrane Technology Research Centre (AMTEC), Block N29a, Universiti Teknologi Malaysia, Skudai 81310, Johor, Malaysia.ORCID 0000-0002-9141-9688
Woei Jye LauAdvanced Membrane Technology Research Centre (AMTEC), Block N29a, Universiti Teknologi Malaysia, Skudai 81310, Johor, Malaysia.ORCID 0000-0002-8581-995X
Nurasyikin MisdanFaculty of Engineering Technology, Universiti Tun Hussein Onn Malaysia (UTHM), Parit Raja, Batu Pahat 86400, Johor, Malaysia.
University of Technology Malaysia · MYTun Hussein Onn University of Malaysia · MYUniversiti Brunei Darussalam · BN

Funding

Advance Membrane Technology Research Centre HICOE A.J091400.5300.07092MRUN Grant Scheme R.J130000.7851.4L865Universiti Teknologi Malaysia HICOE grant scheme R.J090301.7851.4J428UTM Prototype Grant Q.J130000.2851.00L41UTM Shine Grant Scheme Q.J130000.2451.09G21
6 · The paper itself

Abstract

In this current study, facile, one-pot synthesis of functionalised nanocomposite coating with simultaneous hydrophilic and oleophobic properties was successfully achieved via the sol-gel technique. The synthesis of this nanocomposite coating aims to develop a highly efficient, simultaneously oleophobic-hydrophilic coating intended for polymer membranes to spontaneously separate oil-in-water emulsions, therefore, mitigating the fouling issue posed by an unmodified polymer membrane. The simultaneous hydrophilicity-oleophobicity of the nanocoating can be applied onto an existing membrane to improve their capability to spontaneously separate oil-in-water substances in the treatment of oily wastewater using little to no energy and being environmentally friendly. The synthesis of hybrid chitosan-silica (CTS-Si)/halloysite nanotube (HNT) nanocomposite coating using the sol-gel method was presented, and the resultant coating was characterised using FTIR, XPS, XRD, NMR, BET, Zeta Potential, and TGA. The wettability of the nanocomposite coating was evaluated in terms of water and oil contact angle, in which it was coated onto a polymer substrate. The coating was optimised in terms of oil and water contact angle using Response Surface Modification (RSM) with Central Composite Design (CCD) theory. The XPS results revealed the successful grafting of organosilanes groups of HNT onto the CTS-Si denoted by a wide band between 102.6-103.7 eV at Si

Indexed as

chitosan–silica/HNT. hybridhybrid nanocompositenanoparticle coatingssol–gel

Identifiers

PMID36296863
PMCPMC9607117
OpenAlexW4306835783

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.