Evidence map›Paper›PMID 36146034›Full record

ArticlePolymers2022

Analysis of Microplastics in Aquatic Shellfish by Pyrolysis-Gas Chromatography/Mass Spectrometry after Alkali Digestion and Solvent Extraction.

Yingying Zhong, Qibei Bao, Lifeng Yuan, Jiawen Liu, Yan Cai, Xianfeng Chen

Open access · goldAbstract read
In one paragraph

Article in Polymers, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 4 papers.

0numbers the graph read from it
0cells of the map it votes in
4citing papers in PubMed
1.1field-weighted citation impact, top 28% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

4 citing papers in PubMed, 25 citations in OpenAlex.

  1. Review
  2. Article
  3. Article
  4. Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors at 2 institutions in 1 country.

Yingying ZhongNingbo Customs Technology Center, Ningbo 315012, China.ORCID 0000-0002-1202-4048
Qibei BaoNingbo College of Health Sciences, Ningbo 315100, China.
Lifeng YuanNingbo Customs Technology Center, Ningbo 315012, China.
Jiawen LiuCollege of Biology and Environment, Zhejiang Wanli University, Ningbo 315100, China.
Yan CaiCollege of Biology and Environment, Zhejiang Wanli University, Ningbo 315100, China.
Xianfeng ChenNingbo Customs Technology Center, Ningbo 315012, China.
Zhejiang Wanli University · CNNingbo College of Health Sciences · CN

Funding

2021 Science and Technology Innovation Program for College Students cum New Talent Scheme of Zhejiang Province 2021R420013Natural Science Foundation of Ningbo City 202003N4189The General Administration of Customs Scientific Research Program 2020HK207
6 · The paper itself

Abstract

Microplastics are harmful to both marine life and humans. Herein, a pyrolysis-gas chromatography-mass spectrometry (Py-GC/MS) technique for the detection of microplastics in aquatic shellfish is demonstrated. The organic matter in aquatic shellfish was removed by alkali digestion. Subsequently, using hexafluoroisopropanol as the extraction solvent, the extraction method was optimized. The influence of the digestion process on the nature of microplastics was investigated by analyzing the samples before and after the alkali treatment via infrared spectrometry, laser particle sizing, and scanning electron microscopy. Spiked recovery experiments and an analysis of actual samples were performed using PA6 and PA66 as analytes. A quantitative analysis of the characteristic ion fragment produced by high-temperature cracking was performed after chromatographic separation and mass spectrometry identification. The linear range of this method for PA6 and PA66 was 2-64 μg. The limits of detection of PA6 and PA66 were 0.2 and 0.6 μg, while the limits of quantitation were 0.6 and 2.0 μg, respectively. Recovery ranged from 74.4 to 101.62%, with a precision of 4.53-7.56%. The results suggest that the Py-GC/MS technique is suitable for the analysis and detection of trace microplastics in aquatic shellfish.

Indexed as

alkali digestionaquatic shellfishmicroplasticsnylonpyrolysis–gas chromatography–mass spectrometry

Identifiers

PMID36146034
PMCPMC9500840
OpenAlexW4296456619

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.