ArticleNanoscale advances2022
Bottom-up synthesis of 2D layered high-entropy transition metal hydroxides.
Article in Nanoscale advances, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 12 papers.
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Who cites it
12 citing papers in PubMed, 42 citations in OpenAlex.
- Template-Confined Synthesis of 1 nm High-Entropy-Alloy Nanoparticle Library for Electrocatalysis.ACS nano · 2026Article
- Synthesis and Regulation Mechanism of High Entropy Layered Double Hydroxide Electrocatalyst.Small (Weinheim an der Bergstrasse, Germany) · 2026Review
- Multivariate Synergy and Two-Dimensional Confinement: Research Progress and Opportunities of Two-Dimensional High-Entropy Alloys.Precision chemistry · 2026Review
- In Situ Visualization of Electron Beam-Driven High-Entropy Alloy Crystallization.Advanced science (Weinheim, Baden-Wurttemberg, Germany) · 2026Article
- Spinel-Structured High Entropy Oxides: Low Temperature Synthesis, Characterization, and Potential Applications.ACS omega · 2025Article
- Review on the Polymeric and Chelate Gel Precursor for Li-Ion Battery Cathode Material Synthesis.Gels (Basel, Switzerland) · 2024Review
- Zr modulated N doping composites for COiScience · 2024Article
- Synthesis and Thermal Decomposition of High-Entropy Layered Rare Earth Hydroxychlorides.Molecules (Basel, Switzerland) · 2024Article
- Colloidal Nanoparticles of High Entropy Materials: Capabilities, Challenges, and Opportunities in Synthesis and Characterization.ACS nanoscience Au · 2024Review
- Understanding the role of solvents in bottom-up synthesis of multi-element hydroxides.RSC advances · 2024Article
- Development of Two-Dimensional Functional Nanomaterials for Biosensor Applications: Opportunities, Challenges, and Future Prospects.Nanomaterials (Basel, Switzerland) · 2023Review
- Useful High-Entropy Source on Spinel Oxides for Gas Detection.Sensors (Basel, Switzerland) · 2022Article
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Authors and funding
7 authors at 6 institutions in 2 countries.
Funding
No grant is acknowledged in the PubMed record.
Abstract
Low-dimensional high-entropy materials, such as nanoparticles and two-dimensional (2D) layers, have great potential for catalysis and energy applications. However, it is still challenging to synthesize 2D layered high-entropy materials through a bottom-up soft chemistry method, due to the difficulty of mixing and assembling multiple elements in 2D layers. Here, we report a simple polyol process for the synthesis of a series of 2D layered high-entropy transition metal (Co, Cr, Fe, Mn, Ni, and Zn) hydroxides (HEHs), involving the hydrolysis and inorganic polymerization of metal-containing species in ethylene glycol media. The as-synthesized HEHs demonstrate 2D layered structures with interlayer distances ranging from 0.860 to 0.987 nm and homogeneous elemental distribution of designed equimolar stoichiometry in the layers. These 2D HEHs exhibit a low overpotential of 275 mV at 10 mA cm
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