Evidence map›Paper›PMID 36133322›Full record

ArticleNanoscale advances2022

Hierarchically porous and mechanically stable monoliths from ordered mesoporous silica and their water filtration potential.

Laura M Henning, Julian T Müller, Glen J Smales, Brian R Pauw, Johannes Schmidt, Maged F Bekheet, Aleksander Gurlo, Ulla Simon

Abstract read
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Article in Nanoscale advances, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 6 papers.

0numbers the graph read from it
0cells of the map it votes in
6citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

6 citing papers in PubMed.

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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

8 authors.

Laura M HenningTechnische Universität Berlin, Faculty III Process Sciences, Institute of Material Science and Technology, Chair of Advanced Ceramic Materials Straße des 17. Juni 135 10623 Berlin Germany laura.m.henning@ceramics.tu-berlin.de +49 30 314 70483.ORCID https://orcid.org/0000-0003-3989-5908
Julian T MüllerTechnische Universität Berlin, Faculty III Process Sciences, Institute of Material Science and Technology, Chair of Advanced Ceramic Materials Straße des 17. Juni 135 10623 Berlin Germany laura.m.henning@ceramics.tu-berlin.de +49 30 314 70483.ORCID https://orcid.org/0000-0003-0703-8573
Glen J SmalesBundesanstalt für Materialforschung und -prüfung (BAM), Division 6.5 - Polymers in Life Sciences and Nanotechnology Unter den Eichen 87 12205 Berlin Germany glen-jacob.smales@bam.de +49 30 8104 3314.ORCID https://orcid.org/0000-0002-8654-9867
Brian R PauwBundesanstalt für Materialforschung und -prüfung (BAM), Division 6.5 - Polymers in Life Sciences and Nanotechnology Unter den Eichen 87 12205 Berlin Germany glen-jacob.smales@bam.de +49 30 8104 3314.ORCID https://orcid.org/0000-0002-8605-838X
Johannes SchmidtTechnische Universität Berlin, Faculty II Mathematics and Natural Sciences, Institute of Chemistry, Chair of Functional Materials Straße des 17. Juni 135 10623 Berlin Germany.
Maged F BekheetTechnische Universität Berlin, Faculty III Process Sciences, Institute of Material Science and Technology, Chair of Advanced Ceramic Materials Straße des 17. Juni 135 10623 Berlin Germany laura.m.henning@ceramics.tu-berlin.de +49 30 314 70483.ORCID https://orcid.org/0000-0003-1778-0288
Aleksander GurloTechnische Universität Berlin, Faculty III Process Sciences, Institute of Material Science and Technology, Chair of Advanced Ceramic Materials Straße des 17. Juni 135 10623 Berlin Germany laura.m.henning@ceramics.tu-berlin.de +49 30 314 70483.ORCID https://orcid.org/0000-0001-7047-666X
Ulla SimonTechnische Universität Berlin, Faculty III Process Sciences, Institute of Material Science and Technology, Chair of Advanced Ceramic Materials Straße des 17. Juni 135 10623 Berlin Germany laura.m.henning@ceramics.tu-berlin.de +49 30 314 70483.ORCID https://orcid.org/0000-0001-6233-6595

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Mechanically stable structures with interconnected hierarchical porosity combine the benefits of both small and large pores, such as high surface area, pore volume, and good mass transport capabilities. Hence, lightweight micro-/meso-/macroporous monoliths are prepared from ordered mesoporous silica COK-12 by means of spark plasma sintering (SPS, S-sintering) and compared to conventionally (C-) sintered monoliths. A multi-scale model is developed to fit the small angle X-ray scattering data and obtain information on the hexagonal lattice parameters, pore sizes from the macro to the micro range, as well as the dimensions of the silica population. For both sintering techniques, the overall mesoporosity, hexagonal pore ordering, and amorphous character are preserved. The monoliths' porosity (77-49%), mesopore size (6.2-5.2 nm), pore volume (0.50-0.22 g cm

Identifiers

PMID36133322
PMCPMC9470055

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.