Evidence map›Paper›PMID 36051564›Full record

ArticleBeilstein journal of organic chemistry2022

Automated grindstone chemistry: a simple and facile way for PEG-assisted stoichiometry-controlled halogenation of phenols and anilines using

Dharmendra Das, Akhil A Bhosle, Amrita Chatterjee, Mainak Banerjee

Abstract read
In one paragraph

Article in Beilstein journal of organic chemistry, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed.

  1. Dissecting Mechanochemistry III.Beilstein journal of organic chemistry · 2022
    Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

4 authors.

Dharmendra DasDepartment of Chemistry, BITS Pilani, K. K. Birla Goa Campus, Goa 403 726, India.ORCID https://orcid.org/0000-0002-2478-1257
Akhil A BhosleDepartment of Chemistry, BITS Pilani, K. K. Birla Goa Campus, Goa 403 726, India.
Amrita ChatterjeeDepartment of Chemistry, BITS Pilani, K. K. Birla Goa Campus, Goa 403 726, India.ORCID https://orcid.org/0000-0001-8666-2723
Mainak BanerjeeDepartment of Chemistry, BITS Pilani, K. K. Birla Goa Campus, Goa 403 726, India.ORCID https://orcid.org/0000-0002-6833-5531

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

A simple electrical mortar-pestle was used for the development of a green and facile mechanochemical route for the catalyst-free halogenation of phenols and anilines via liquid-assisted grinding using PEG-400 as the grinding auxiliary. A series of mono-, di-, and tri-halogenated phenols and anilines was synthesized in good to excellent yields within 10-15 min in a chemoselective manner by controlling the stoichiometry of

Indexed as

automated grindingchemoselectivitymechanochemistryN-bromosuccinimidePEG-400regioselectivitystoichiometry-controlled halogenation

Identifiers

PMID36051564
PMCPMC9379637

What OpenQuestion holds

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LicenceCC BY
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Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.