Evidence map›Paper›PMID 36034652›Full record

ArticleFrontiers in chemistry2022

Development of a reliable UHPLC-MS/MS method for simultaneous determination of zearalenone and zearalenone-14-glucoside in various feed products.

Zhiqi Zhang, Yaling Cai, Kai Fan, Qingwen Huang, Xiuying Zhao, Haojie Cao, Zhihui Zhao, Emmanuel K Tangni, Zheng Han

Abstract read
PubMed Full text at PMC Publisher
In one paragraph

Article in Frontiers in chemistry, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Article
  2. Toxins · 2026
    Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

9 authors.

Zhiqi ZhangInstitute for Agro-Food Standards and Testing Technology, Shanghai Academy of Agricultural Sciences, Shanghai, China.
Yaling CaiInstitute for Agro-Food Standards and Testing Technology, Shanghai Academy of Agricultural Sciences, Shanghai, China.
Kai FanInstitute for Agro-Food Standards and Testing Technology, Shanghai Academy of Agricultural Sciences, Shanghai, China.
Qingwen HuangInstitute for Agro-Food Standards and Testing Technology, Shanghai Academy of Agricultural Sciences, Shanghai, China.
Xiuying ZhaoInstitute for Agro-Food Standards and Testing Technology, Shanghai Academy of Agricultural Sciences, Shanghai, China.
Haojie CaoInstitute for Agro-Food Standards and Testing Technology, Shanghai Academy of Agricultural Sciences, Shanghai, China.
Zhihui ZhaoInstitute for Agro-Food Standards and Testing Technology, Shanghai Academy of Agricultural Sciences, Shanghai, China.
Emmanuel K TangniOrganic Contaminants and Additives, Chemical and Physical Health Risks, Brussels, Belgium.
Zheng HanInstitute for Agro-Food Standards and Testing Technology, Shanghai Academy of Agricultural Sciences, Shanghai, China.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

A reliable ultra-high-performance liquid chromatography-tandem mass spectrometry method (UHPLC-MS/MS) was developed for the simultaneous determination of two mycotoxins, that is, zearalenone (ZEN) and zearalenone-14-glucoside (ZEN-14G) in formula feed, concentrated feed, and premixed feed products. An improved sample pretreatment was achieved with the hydrophilic-lipophilic balance (HLB) cartridges efficiently removing the impurities and enriching the target analytes in different feeds. The critical parameters affecting the performance of the solid-phase extraction (SPE) procedure were carefully optimized, and 20% acetonitrile in water as the loading solution, 50% methanol in water as the washing solvent, and 5 ml of methanol as the elution solvent yielded the optimal purification efficiencies. The established method was thoroughly validated in terms of linearity (

Indexed as

feed productsHLB cartridgesultra-high-performance liquid chromatography–tandem mass spectrometryzearalenonezearalenone-14-glucoside

Identifiers

PMID36034652
PMCPMC9399508

What OpenQuestion holds

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LicenceCC BY
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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.