Evidence map›Paper›PMID 35957072›Full record

ArticleNanomaterials (Basel, Switzerland)2022

Physicochemical Characterization and Finite Element Analysis-Assisted Mechanical Behavior of Polylactic Acid-Montmorillonite 3D Printed Nanocomposites.

Maria-Eirini Grigora, Zoe Terzopoulou, Konstantinos Tsongas, Dimitrios N Bikiaris, Dimitrios Tzetzis

Abstract read
In one paragraph

Article in Nanomaterials (Basel, Switzerland), 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 8 papers.

0numbers the graph read from it
0cells of the map it votes in
8citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

8 citing papers in PubMed.

  1. Review
  2. Article
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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

5 authors.

Maria-Eirini GrigoraDigital Manufacturing and Materials Characterization Laboratory, School of Science and Technology, International Hellenic University, 57001 Thessaloniki, Greece.ORCID 0000-0002-4985-0773
Zoe TerzopoulouLaboratory of Polymer Chemistry and Technology, Department of Chemistry, Aristotle University of Thessaloniki, 54124 Thessaloniki, Greece.ORCID 0000-0001-7935-2145
Konstantinos TsongasDigital Manufacturing and Materials Characterization Laboratory, School of Science and Technology, International Hellenic University, 57001 Thessaloniki, Greece.ORCID 0000-0001-7050-5432
Dimitrios N BikiarisLaboratory of Polymer Chemistry and Technology, Department of Chemistry, Aristotle University of Thessaloniki, 54124 Thessaloniki, Greece.ORCID 0000-0001-8458-4952
Dimitrios TzetzisDigital Manufacturing and Materials Characterization Laboratory, School of Science and Technology, International Hellenic University, 57001 Thessaloniki, Greece.ORCID 0000-0001-5006-5759

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

This work aims to improve the properties of poly(lactic acid) (PLA) for future biomedical applications by investigating the effect of montmorillonite (MMT) nanoclay on physicochemical and mechanical behavior. PLA nanocomposite filaments were fabricated using different amounts of MMT (1.0, 2.0, and 4.0 wt.%) and 2 wt.% Joncryl chain extenders. The 3D-printed specimens were manufactured using Fused Filament Fabrication (FFF). The composites were characterized by Gel Permeation Chromatography (GPC), Melt Flow Index (MFI), X-ray Diffraction (XRD), and Fourier-transform infrared spectroscopy (FTIR). The thermal properties were studied by means of Differential Scanning Calorimetry (DSC) and Thermogravimetric Analysis (TGA). Moreover, the hydrophilicity of the PLA/MMT nanocomposites was investigated by measuring the water contact angle. The mechanical behavior of the PLA/MMT nanocomposites was examined with nanoindentation, compression tests, and Dynamic Mechanical Analysis (DMA). The presence of Joncryl, as well as the pretreatment of MMT before filament fabrication, improved the MMT distribution in the nanocomposites. Furthermore, MMT enhanced the printability of PLA and improved the hydrophilicity of its surface. In addition, the results of nanoindentation testing coupled with Finite Element Analysis showed that as the MMT weight fraction increased, as well as an increased Young's modulus. According to the results of the mechanical analysis, the best mechanical behavior was achieved for PLA nanocomposite with 4 wt.% MMT.

Indexed as

compressionFEAFused Filament Fabricationmontmorillonitenanocompositesnanoindentationpoly(lactic acid)

Identifiers

PMID35957072
PMCPMC9370662

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.