ArticleJournal of the American Chemical Society2022
Direct Location of Organic Molecules in Framework Materials by Three-Dimensional Electron Diffraction.
Article in Journal of the American Chemical Society, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 11 papers.
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Who cites it
11 citing papers in PubMed.
- Automated Nanocrystalline Sponge Workflow Enabled by 3D Electron Diffraction.Journal of the American Chemical Society · 2026Article
- Multimodal Nanoscale Mapping of Local Structure and COJournal of the American Chemical Society · 2026Article
- Low-Dimensional Zeotypes Templated by Stacked Cyclic Benzimidazolium Revealed by Electron Crystallography.Journal of the American Chemical Society · 2026Article
- Open Framework Structure of the New Pure-Germania Zeolite ITQ-35 Solved by 3D Electron Diffraction.Small methods · 2025Article
- Localized Boron Sites in Large Pore Borosilicate Zeolite EMM-59 Determined by Electron Crystallography.Journal of the American Chemical Society · 2024Article
- Single-Crystal Structural Analysis of 2D Metal-Organic Frameworks and Covalent Organic Frameworks by Three-Dimensional Electron Diffraction.Accounts of chemical research · 2024Article
- Article
- Applying 3D ED/MicroED workflows toward the next frontiers.Acta crystallographica. Section C, Structural chemistry · 2024Article
- Advances and applications of microcrystal electron diffraction (MicroED).Current opinion in structural biology · 2024Review
- Structure determination of a low-crystallinity covalent organic framework by three-dimensional electron diffraction.Communications chemistry · 2023Article
- Improving data quality for three-dimensional electron diffraction by a post-column energy filter and a new crystal tracking method.Journal of applied crystallography · 2022Article
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Authors and funding
5 authors.
Funding
No grant is acknowledged in the PubMed record.
Abstract
In the study of framework materials, probing interactions between frameworks and organic molecules is one of the most important tasks, which offers us a fundamental understanding of host-guest interactions in gas sorption, separation, catalysis, and framework structure formation. Single-crystal X-ray diffraction (SCXRD) is a conventional method to locate organic species and study such interactions. However, SCXRD demands large crystals whose quality is often vulnerable to, e.g., cracking on the crystals by introducing organic molecules, and this is a major challenge to use SCXRD for structural analysis. With the development of three-dimensional electron diffraction (3D ED), single-crystal structural analysis can be performed on very tiny crystals with sizes on the nanometer scale. Here, we analyze two framework materials, SU-8 and SU-68, with organic molecules inside their inorganic crystal structures. By applying 3D ED, with fast data collection and an ultralow electron dose (0.8-2.6 e
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Registered trials
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