ArticleFrontiers in nutrition2022
Rapid determination of 103 common veterinary drug residues in milk and dairy products by ultra performance liquid chromatography tandem mass spectrometry.
Article in Frontiers in nutrition, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 13 papers.
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13 citing papers in PubMed.
- Suspected and Non-Targeted Screening of Non-Edible Substances in Food by UPLC-Q-TOF-MS.Foods (Basel, Switzerland) · 2026Article
- Biomass tomato pomace as a fluorescence probe for determination of toltrazuril in veterinary pharmaceuticals and milk samples.BMC chemistry · 2026Article
- Article
- Recent Advances in Pretreatment Methods and Detection Techniques for Veterinary Drug Residues in Animal-Derived Foods.Metabolites · 2025Review
- FeRSC advances · 2025Article
- Electrochemical biosensor for detection of ampicillin in milk based on AuMikrochimica acta · 2024Article
- Dairy Chain Safety in the Context of Antibiotic Residues-Current Status of Confirmatory Liquid Chromatography Methods: A Review.Antibiotics (Basel, Switzerland) · 2024Review
- [Determination of five veterinary drug residues in milk by ultra-high performance liquid chromatography-quadrupole/electrostatic field orbitrap mass spectrometry based on modified chitosan membrane purification].Se pu = Chinese journal of chromatography · 2024Article
- A modified QuEChERS-based UPLC-MS/MS method for rapid determination of multiple antibiotics and sedative residues in freshwater fish.Food chemistry: X · 2024Article
- Recent Advances in the Chromatographic Analysis of Emerging Pollutants in Dairy Milk: A Review (2018-2023).Molecules (Basel, Switzerland) · 2024Review
- Dispersive Solid-Phase Extraction and Ultra-Performance Liquid Chromatography-Tandem Mass Spectrometry-A Rapid and Accurate Method for Detecting 10 Macrolide Residues in Aquatic Products.Foods (Basel, Switzerland) · 2024Article
- What Are We Eating? Surveying the Presence of Toxic Molecules in the Food Supply Chain Using Chromatographic Approaches.Molecules (Basel, Switzerland) · 2024Review
- Determination of Multiclass Pharmaceutical Residues in Milk Using Modified QuEChERS and Liquid-Chromatography-Hybrid Linear Ion Trap/Orbitrap Mass Spectrometry: Comparison of Clean-Up Approaches and Validation Studies.Molecules (Basel, Switzerland) · 2023Article
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8 authors.
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Abstract
A multi-residue method has been developed for the identification and quantification of 103 common veterinary drug residues in milk and dairy Products. This method was based on QuEChERS with dispersive solid-phase where C18 sorbent and anhydrous sodium sulfate were used to sample purification. After evaporation and reconstitution, the samples were analyzed by ultra-performance liquid chromatography-tandem mass spectrometry. The mean recovery results were all higher than 60% except ampicillin, pipemidic acid, enoxacin, and estriol, and the relative standard deviation was <20.0%. The limit of quantification ranged between 0.1 and 5 μg/kg for milk and between 0.5 and 25 μg/kg for milk powder. It was successfully used to detect residues of veterinary drug in real samples. This study proposes a simple and fast analytical method for monitoring multi-class veterinary drug residues to ensure food safety.
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