Pulsed-sonochemiluminescence combined with molecularly imprinted polymerized high internal phase emulsion adsorbent for determination of bentazone.

Zohreh Akbarzadeh, Ali Mokhtari, Ghasem Bahlakeh, Hossein Karimian

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Article in Mikrochimica acta, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

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4 authors.

Zohreh AkbarzadehDepartment of Chemistry, Faculty of Sciences, Golestan University, PO Box 4936179142, Gorgan, Iran.

Ali MokhtariDepartment of Chemistry, Faculty of Sciences, Golestan University, PO Box 4936179142, Gorgan, Iran. a.mokhtari@gu.ac.ir.ORCID http://orcid.org/0000-0003-4783-3467

Ghasem BahlakehDepartment of Chemical Engineering, Faculty of Engineering, Golestan University, Aliabad Katoul, Iran.

Hossein KarimianDepartment of Chemical Engineering, Faculty of Engineering, Golestan University, Aliabad Katoul, Iran.

Funding

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6 · The paper itself

Abstract

A small low-power humidifier with a simple programmable on/off switch was used as a pulsed ultrasound generator. Using this tool, a novel sonochemiluminescence (SCL) method was developed to determine bentazone. To the best of our knowledge, no chemiluminescence method has been proposed to determine this pesticide. Only five studies have been proposed for SCL quantitative applications so far. Therefore, revealing new aspects of SCL promises to develop analytical methods for the quantitative determination of different substances. A molecularly imprinted polymerized high internal phase emulsion (MIP-polyHIPE) was synthesized, bentazone separated from aqueous solutions, and pre-concentrated by the MIP-polyHIPE foam. The adsorption of bentazone on the MIP-polyHIPE adsorbent was theoretically studied by density functional theory through molecular dynamics simulation. Both experimental and simulation results indicated removal and pre-concentration of bentazone by the MIP-polyHIPE adsorbent. Using the proposed SCL method and without pre-concentration process, a linear dynamic range (LDR) of 2.5 × 10

Indexed as

Molecular ImprintingBenzothiadiazinesEmulsionsPolymerizationWaterbentazoneBenzothiadiazinesEmulsionsWaterBentazoneDensity functional theoryHigh internal phase emulsion adsorbentsMolecular dynamics simulationMolecularly imprinted polymerSonochemiluminescence

Identifiers

PMID35913687

DOI10.1007/s00604-022-05406-2

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