Evidence map›Paper›PMID 35879427›Full record

ArticleAnalytical and bioanalytical chemistry2022

Improved method for the determination of endocrine-disrupting chemicals in urine of school-age children using microliquid-liquid extraction and UHPLC-MS/MS.

Inmaculada Moscoso-Ruiz, Yolanda Gálvez-Ontiveros, María Giles-Mancilla, María Del Carmen Gómez-Regalado, Ana Rivas, Alberto Zafra-Gómez

Abstract read
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In one paragraph

Article in Analytical and bioanalytical chemistry, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 8 papers.

0numbers the graph read from it
0cells of the map it votes in
8citing papers in PubMed
1.4field-weighted citation impact, top 21% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

8 citing papers in PubMed, 14 citations in OpenAlex.

  1. Review
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  6. Risk assessment of food contact materials.EFSA journal. European Food Safety Authority · 2023
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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors at 2 institutions in 1 country.

Inmaculada Moscoso-RuizDepartment of Analytical Chemistry, University of Granada, 18071, Granada, Spain.
Yolanda Gálvez-OntiverosDepartment of Nutrition and Food Science, University of Granada, 18071, Granada, Spain.
María Giles-MancillaDepartment of Nutrition and Food Science, University of Granada, 18071, Granada, Spain.
María Del Carmen Gómez-RegaladoDepartment of Analytical Chemistry, University of Granada, 18071, Granada, Spain.
Ana RivasDepartment of Nutrition and Food Science, University of Granada, 18071, Granada, Spain.
Alberto Zafra-GómezDepartment of Analytical Chemistry, University of Granada, 18071, Granada, Spain. azafra@ugr.es.
Instituto de Investigación Biosanitaria de Granada · ESUniversidad de Granada · ES

Funding

Andalusia Government P18-RT-4247Andalusia Government PE-0250-2019Spanish Government FEDER-ISCIII PI20/01278Spanish Ministry of Education, Culture and Sports FPU19/05989
6 · The paper itself

Abstract

The presence of endocrine-disrupting chemicals in our daily life is increasing every day and, by extension, human exposure and the consequences thereof. Among these substances are bisphenols and parabens. Urine is used to analyze the exposure. The determination of 12 bisphenol homologues and 6 parabens is proposed. A procedure based on a method previously developed by our research group in 2014 is improved. The extraction yield is higher, because the new protocol is 5 times more efficient. Also, a comparison between calibration with pure standards and matrix calibration, to calculate the matrix effect, was also made. A high grade of matrix effect for all analytes was observed. In terms of validation, the limits of detection (LOD) were between 0.03 and 0.3 ng mL

Indexed as

Endocrine DisruptorsTandem Mass SpectrometryChildChromatography, High Pressure LiquidHumansLimit of DetectionParabensEndocrine DisruptorsParabensBisphenolsDispersive liquid–liquid microextractionEndocrine-disrupting chemicalsParabensUHPLC-MS/MSUrine samples

Identifiers

PMID35879427
OpenAlexW4287831653

What OpenQuestion holds

Textmetadata
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.