Evidence map›Paper›PMID 35855986›Full record

ArticleHeliyon2022

A facile approach for the determination of degree of deacetylation of chitosan using acid-base titration.

Joydeep Dutta, Priyanka

Abstract read
In one paragraph

Article in Heliyon, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 12 papers.

0numbers the graph read from it
0cells of the map it votes in
12citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

12 citing papers in PubMed.

  1. Article
  2. Article
  3. Article
  4. Article
  5. Article
  6. Article
  7. Article
  8. Review
  9. Article
  10. Review
  11. Article
  12. Isolation and screening of a chitin deacetylase producingFrontiers in bioengineering and biotechnology · 2023
    Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

2 authors.

Joydeep DuttaDepartment of Chemistry, Amity School of Applied Sciences, Amity University Haryana, Gurgaon 122413, Haryana, India.
PriyankaDepartment of Chemistry, Amity School of Applied Sciences, Amity University Haryana, Gurgaon 122413, Haryana, India.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Several spectroscopic techniques such as nuclear magnetic resonance (NMR), UV-visible, Fourier transform infrared (FT-IR), etc. have been already used for the determination of degree of deacetylation (DD) of chitosan. These techniques involve the interpretation of spectral data apart from sample preparation for obtaining DD of chitosan. In addition, inaccurate interpretation of data sometimes misleads researchers to get an exact value of DD of chitosan. Among them, NMR is an excellent technique for the estimation of DD of chitosan but expensive and not found easily in every research laboratory. On the other hand, titrimetric methods have been employed by many researchers for determining the DD of chitosan but these existing methods involve many complex calculations, which do not always give accurate results. Moreover, few of the acid-base titration methods are little complicated for execution. Therefore, in this present study, we adopted a very handy and simple acid-base titration method with a new approach and proposed a new equation facilitating the ease of calculation that is not reported elsewhere for the determination of DD value by observing the net volume of NaOH consumed for the complete neutralization of protonated amino groups (-NH

Indexed as

13C-NMRAcid-base titrationChitosanDegree of deacetylationEase of calculationNew equation

Identifiers

PMID35855986
PMCPMC9287797

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.