Evidence map›Paper›PMID 35745908›Full record

ArticlePolymers2022

Cenospheres-Reinforced PA-12 Composite: Preparation, Physicochemical Properties, and Soaking Tests.

Damian S Nakonieczny, Magdalena Antonowicz, Thomas Heim, Andrzej S Swinarew, Paweł Nuckowski, Krzysztof Matus, Marcin Lemanowicz

Open access · goldAbstract read
PubMed Full text at PMC Publisher
In one paragraph

Article in Polymers, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
0.7field-weighted citation impact, top 37% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed, 8 citations in OpenAlex.

  1. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

7 authors at 3 institutions in 2 countries.

Damian S NakoniecznyInstitute for Manufacturing Technologies of Ceramic Components and Composites, University of Stuttgart, 70569 Stuttgart, Germany.ORCID 0000-0001-6882-2930
Magdalena AntonowiczDepartment of Biomedical Engineering, Silesian University of Technology, Akademicka 2A, 44-100 Gliwice, Poland.ORCID 0000-0001-5755-490X
Thomas HeimInstitute for Manufacturing Technologies of Ceramic Components and Composites, University of Stuttgart, 70569 Stuttgart, Germany.
Andrzej S SwinarewFaculty of Science and Technology, University of Silesia in Katowice, 41-500 Chorzów, Poland.ORCID 0000-0001-6116-9510
Paweł NuckowskiMaterials Research Laboratory, Faculty of Mechanical Engineering, Silesian University of Technology, Konarskiego 18 A, 44-100 Gliwice, Poland.ORCID 0000-0002-2606-0525
Krzysztof MatusMaterials Research Laboratory, Faculty of Mechanical Engineering, Silesian University of Technology, Konarskiego 18 A, 44-100 Gliwice, Poland.ORCID 0000-0002-4015-5600
Marcin LemanowiczFaculty of Chemistry, Department of Chemical Engineering and Process Design, Silesian University of Technology, Akademicka 2A, 44-100 Gliwice, Poland.ORCID 0000-0002-1679-6221
Silesian University of Technology · PLUniversity of Stuttgart · DEAkademii Wychowania Fizycznego im. Jerzego Kukuczki w Katowicach · PL

Funding

Polish National Centre of Science 2019/03/X/ST5/00042Rector's Habilitation Grant. The Silesian University of Technology 07/020/RGH20/0062
6 · The paper itself

Abstract

The main aim of this research was the preparation of a polymer-ceramic composite with PA-12 as the polymer matrix and modified aluminosilicate cenospheres (CSs) as the ceramic filler. The CSs were subjected to an early purification and cleaning process, which was also taken as a second objective. The CSs were surface modified by a two-step process: (1) etching in Piranha solution and (2) silanization in 3-aminopropyltriethoxysilane. The composite was made for 3D printing by FDM. Raw and modified CSs and a composite with PA-12 were subjected to the following tests: surface development including pores (BET), real density (HP), chemical composition and morphology (SEM/EDS, FTIR), grain analysis (PSD), phase composition (XRD), hardness (HV), and static tensile tests. The composites were subjected to soaking under simulated body fluid (SBF) conditions in artificial saliva for 14, 21, and 29 days. Compared to pure PA-12, PA-12_CS had generally better mechanical properties and was more resistant to SBF at elevated temperatures and soaking times. These results showed this material has potential for use in biomedical applications. These results also showed the necessity of developing a kinetic aging model for aging in different liquids to verify the true value of this material.

Indexed as

APTEScenospherescompositesPiranha solutionpolyamide PA-12surface modification

Identifiers

PMID35745908
PMCPMC9229177
OpenAlexW4282551737

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.