Evidence map›Paper›PMID 35719303›Full record

ArticleJournal of applied crystallography2022

3D-printed equipment to decouple (powder) X-ray diffraction sample preparation and measurement.

Friederike Fuß, Max Rieckert, Simon Steinhauer, Moritz Liesegang, Günther Thiele

Abstract read
In one paragraph

Article in Journal of applied crystallography, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Optical and Electrical Properties of AInorganic chemistry · 2024
    Article
  2. Compression Strength of PLA Bolts Produced via FDM.Materials (Basel, Switzerland) · 2022
    Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

5 authors.

Friederike FußFachbereich Biologie Chemie Pharmazie, Freie Universität Berlin, Fabeckstraße 34-36, Berlin, 14195, Germany.ORCID https://orcid.org/0000-0003-3829-8968
Max RieckertFachbereich Biologie Chemie Pharmazie, Freie Universität Berlin, Fabeckstraße 34-36, Berlin, 14195, Germany.ORCID https://orcid.org/0000-0003-1766-8368
Simon SteinhauerFachbereich Biologie Chemie Pharmazie, Freie Universität Berlin, Fabeckstraße 34-36, Berlin, 14195, Germany.
Moritz LiesegangInstitut für Geologische Wissenschaften, Mineralogie-Petrologie, Freie Universität Berlin, Malteserstraße 74-100, Berlin, 12249, Germany.ORCID https://orcid.org/0000-0002-5363-4248
Günther ThieleFachbereich Biologie Chemie Pharmazie, Freie Universität Berlin, Fabeckstraße 34-36, Berlin, 14195, Germany.ORCID https://orcid.org/0000-0003-2935-9335

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

An alternative storage method to separate sample preparation from single-crystal and powder X-ray diffraction measurements at home source diffractometers is described. For single crystals, a setup is presented which allows storage of preselected crystals under cryogenic and ambient temperatures. For powders, a disposable sample holder is introduced. The method is suitable for the storage of air- and moisture-sensitive samples. Equipment made of biodegradable polylactic acid is produced by 3D printing and can be adapted to individual needs. As 3D printers are widely available at research institutions nowadays, models of the presented equipment are provided for the reader to allow easy reproduction.

Indexed as

3D printingcryo-storagediffractionhome sourcespowderssingle crystals

Identifiers

PMID35719303
PMCPMC9172037

What OpenQuestion holds

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LicenceCC BY
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Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.