Evidence map›Paper›PMID 35682585›Full record

ArticleInternational journal of molecular sciences2022

Molecular Level Characterisation of the Surface of Carbohydrate-Functionalised

Karolina Krajewska, Anna M Gołkowska, Maciej Nowak, Marta Kozakiewicz-Latała, Wojciech Pudło, Andrzej Żak, Bożena Karolewicz, Yaroslav Z Khimyak, Karol P Nartowski

Abstract read
In one paragraph

Article in International journal of molecular sciences, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 3 papers.

0numbers the graph read from it
0cells of the map it votes in
3citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

3 citing papers in PubMed.

  1. Review
  2. Article
  3. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

9 authors.

Karolina KrajewskaDepartment of Drug Form Technology, Wroclaw Medical University, Borowska 211A, 50-556 Wroclaw, Poland.ORCID 0000-0002-5338-5309
Anna M GołkowskaDepartment of Drug Form Technology, Wroclaw Medical University, Borowska 211A, 50-556 Wroclaw, Poland.ORCID 0000-0003-4422-1246
Maciej NowakDepartment of Drug Form Technology, Wroclaw Medical University, Borowska 211A, 50-556 Wroclaw, Poland.ORCID 0000-0002-7656-7244
Marta Kozakiewicz-LatałaDepartment of Drug Form Technology, Wroclaw Medical University, Borowska 211A, 50-556 Wroclaw, Poland.ORCID 0000-0001-8822-126X
Wojciech PudłoDepartment of Chemical Engineering and Process Design, Silesian University of Technology, M. Strzody 7 Str., 44-100 Gliwice, Poland.
Andrzej ŻakFaculty of Mechanical Engineering, Wroclaw University of Science and Technology (WUST), Wybrzeze Wyspianskiego 27, 50-370 Wroclaw, Poland.ORCID 0000-0002-4512-2816
Bożena KarolewiczDepartment of Drug Form Technology, Wroclaw Medical University, Borowska 211A, 50-556 Wroclaw, Poland.ORCID 0000-0003-0970-6344
Yaroslav Z KhimyakSchool of Pharmacy, University of East Anglia, Norwich Research Park, Norwich NR4 7TJ, UK.
Karol P NartowskiDepartment of Drug Form Technology, Wroclaw Medical University, Borowska 211A, 50-556 Wroclaw, Poland.

Funding

Ministry of Science and Higher Education in Poland SUBK.D190.22.022
6 · The paper itself

Abstract

Atomistic level characterisation of external surface species of mesoporous silica nanoparticles (MSN) poses a significant analytical challenge due to the inherently low content of grafted ligands. This study proposes the use of HR-MAS NMR spectroscopy for a molecular level characterisation of the external surface of carbohydrate-functionalised nanoparticles. MSN differing in size (32 nm, 106 nm, 220 nm) were synthesised using the sol-gel method. The synthesised materials displayed narrow particle size distribution (based on DLS and TEM results) and a hexagonal arrangement of the pores with a diameter of ca. 3 nm as investigated with PXRD and N

Indexed as

NanoparticlesSilicon DioxideDrug Delivery SystemsLactoseMagnetic Resonance SpectroscopyPorosityLactoseSilicon DioxidefunctionalisationHR-MAS NMRmesoporous silica nanoparticlesMSNNMRporous materialssurface

Identifiers

PMID35682585
PMCPMC9180545

What OpenQuestion holds

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Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.