ArticleAngewandte Chemie (International ed. in English)2022
The Direct Mechanocatalytic Suzuki-Miyaura Reaction of Small Organic Molecules.
Article in Angewandte Chemie (International ed. in English), 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 15 papers.
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Who cites it
15 citing papers in PubMed.
- The role of ball mass, surface, and contact dynamics in mechanochemical reactions.RSC mechanochemistry · 2026Article
- Motion matters: the role of milling ball trajectories in mechanochemical reactions.RSC mechanochemistry · 2026Article
- Experimental Isolation of Single Impact, Cumulative Energy, Aging, and Liquid-Assisted Grinding Effects in Mechanochemical Reactions.Angewandte Chemie (International ed. in English) · 2026Article
- Article
- Mechanochemical Strategies Applied to the Late-Stage Modifications of Pharmaceutically Active Compounds.Angewandte Chemie (International ed. in English) · 2025Review
- Solid-State Photochemistry in Resonant Acoustic Mixers.Chemistry (Weinheim an der Bergstrasse, Germany) · 2025Article
- Thermally accelerated Heck reaction under direct mechanocatalysis using palladium milling balls.RSC mechanochemistry · 2025Article
- Advances in Mechanochemical Methods for One-Pot Multistep Organic Synthesis.Chemistry (Weinheim an der Bergstrasse, Germany) · 2025Review
- Liquid palladium for high-turnover carbon-carbon bond formation.Science advances · 2025Article
- Article
- Upcycling of Chitin to Cross-Coupling Catalysts: Tailored Supports and Opportunities in Mechanochemistry.ChemSusChem · 2025Article
- Direct mechanocatalysis by resonant acoustic mixing (RAM).Chemical science · 2023Article
- From Inert to Catalytically Active Milling Media: Galvanostatic Coating for Direct Mechanocatalysis.Angewandte Chemie (International ed. in English) · 2022Article
- Article
- The Direct Mechanocatalytic Suzuki-Miyaura Reaction of Small Organic Molecules.Angewandte Chemie (International ed. in English) · 2022Article
Corrections and comments
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Authors and funding
8 authors.
Funding
Abstract
The molecular Suzuki cross-coupling reaction was conducted mechanochemically, without solvents, ligands, or catalyst powders. Utilizing one catalytically active palladium milling ball, products could be formed in quantitative yield in as little as 30 min. In contrast to previous reports, the adjustment of milling parameters led to the complete elimination of abrasion from the catalyst ball, thus enabling the first reported systematic catalyst analysis. XPS, in situ XRD, and reference experiments provided evidence that the milling ball surface was the location of the catalysis, allowing a mechanism to be proposed. The versatility of the approach was demonstrated by extending the substrate scope to deactivated and even sterically hindered aryl iodides and bromides.
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Registered trials
Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.