Evidence map›Paper›PMID 35614129›Full record

ArticleScientific data2022

Dataset of solution-based inorganic materials synthesis procedures extracted from the scientific literature.

Zheren Wang, Olga Kononova, Kevin Cruse, Tanjin He, Haoyan Huo, Yuxing Fei, Yan Zeng, Yingzhi Sun, Zijian Cai, Wenhao Sun and 1 more

Abstract read
In one paragraph

Article in Scientific data, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 18 papers.

0numbers the graph read from it
0cells of the map it votes in
18citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

18 citing papers in PubMed.

  1. Review
  2. Article
  3. Article
  4. Review
  5. Article
  6. Article
  7. Steering towards safe self-driving laboratories.Nature reviews. Chemistry · 2025
    Review
  8. Article
  9. Article
  10. Intelligent Systems for Inorganic Nanomaterial Synthesis.Nanomaterials (Basel, Switzerland) · 2025
    Review
  11. Article
  12. Article
  13. Article
  14. Text Mining the Literature to Inform Experiments and Rationalize Impurity Phase Formation for BiFeOChemistry of materials : a publication of the American Chemical Society · 2024
    Article
  15. Article
  16. Machine-Learning Rationalization and Prediction of Solid-State Synthesis Conditions.Chemistry of materials : a publication of the American Chemical Society · 2022
    Article
  17. Article
  18. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

11 authors.

Zheren WangDepartment of Materials Science and Engineering, University of California, Berkeley, CA, 94720, USA.
Olga KononovaDepartment of Materials Science and Engineering, University of California, Berkeley, CA, 94720, USA.ORCID 0000-0001-9267-312X
Kevin CruseDepartment of Materials Science and Engineering, University of California, Berkeley, CA, 94720, USA.
Tanjin HeDepartment of Materials Science and Engineering, University of California, Berkeley, CA, 94720, USA.ORCID 0000-0001-8834-8703
Haoyan HuoDepartment of Materials Science and Engineering, University of California, Berkeley, CA, 94720, USA.ORCID 0000-0003-2227-9121
Yuxing FeiDepartment of Materials Science and Engineering, University of California, Berkeley, CA, 94720, USA.
Yan ZengMaterials Sciences Division, Lawrence Berkeley National Laboratory, Berkeley, CA, 94720, USA.
Yingzhi SunDepartment of Materials Science and Engineering, University of California, Berkeley, CA, 94720, USA.ORCID 0000-0003-3559-6863
Zijian CaiDepartment of Materials Science and Engineering, University of California, Berkeley, CA, 94720, USA.
Wenhao SunDepartment of Materials Science and Engineering, University of Michigan, Ann Arbor, MI, USA.ORCID 0000-0002-8416-455X
Gerbrand CederDepartment of Materials Science and Engineering, University of California, Berkeley, CA, 94720, USA. gceder@berkeley.edu.ORCID 0000-0001-9275-3605

Funding

National Science Foundation (NSF) DMR-1922372
6 · The paper itself

Abstract

The development of a materials synthesis route is usually based on heuristics and experience. A possible new approach would be to apply data-driven approaches to learn the patterns of synthesis from past experience and use them to predict the syntheses of novel materials. However, this route is impeded by the lack of a large-scale database of synthesis formulations. In this work, we applied advanced machine learning and natural language processing techniques to construct a dataset of 35,675 solution-based synthesis procedures extracted from the scientific literature. Each procedure contains essential synthesis information including the precursors and target materials, their quantities, and the synthesis actions and corresponding attributes. Every procedure is also augmented with the reaction formula. Through this work, we are making freely available the first large dataset of solution-based inorganic materials synthesis procedures.

Identifiers

PMID35614129
PMCPMC9132903

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.