Evidence map›Paper›PMID 35541648›Full record

ArticleRSC advances2018

Perfecting band selective homo-decoupling for decoupling two signals coupled within the same band.

Ajay Verma, Subrato Bhattacharya, Bikash Baishya

Abstract read
In one paragraph

Article in RSC advances, 2018. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

0numbers the graph read from it
0cells of the map it votes in
0citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

0 citing papers in PubMed.

No citing paper in PubMed yet.

4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

3 authors.

Ajay VermaCentre of Biomedical Research SGPGIMS Campus, RaeBareli Road Lucknow-226014 U.P. India bikashbaishya@gmail.com +91-522-2668215.
Subrato BhattacharyaDepartment of Chemistry, Institute of Science, Banaras Hindu University Banaras-221005 U.P. India.
Bikash BaishyaCentre of Biomedical Research SGPGIMS Campus, RaeBareli Road Lucknow-226014 U.P. India bikashbaishya@gmail.com +91-522-2668215.ORCID https://orcid.org/0000-0002-4669-6600

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Recently, pure shift NMR methods have delivered ultrahigh resolution broadband proton NMR spectra that display singlet peak per chemical site. BASH/HOBS (band selective homo-decoupling/homonuclear band selective) decoupling is the only method that provides singlet only spectrum for a selected signal or a group of signals with a sensitivity higher than regular proton NMR, and an order of magnitude higher than broadband pure shift techniques. It is this aspect that makes this technique important. In the present work, we show that perfect echo (PE) when combined with band selective homo-decoupling (BASHD) permits increasing the bandwidth of the BASH/HOBS decoupling resulting in reduced experimental time for this class of experiments. Using new PE-BASHD technique two closely resonating coupled signals could be decoupled in a single experiment which otherwise demands two separate BASHD experiments. In polypeptides, it also allows decoupling of H

Identifiers

PMID35541648
PMCPMC9080728

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.