Evidence map›Paper›PMID 35531408›Full record

ArticleJournal of food science and technology2022

Improved chromatographic performance in red chilli powder pesticide residue quantitation by retention gap introduction in gas chromatography tandem mass spectrometry.

Chandrasekar Kandaswamy, Davis Presley, T P Shabeer Ahammed, Sreekanth Anadaram

Open access · greenAbstract read
In one paragraph

Article in Journal of food science and technology, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
0.3field-weighted citation impact, top 38% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed, 4 citations in OpenAlex.

  1. Article
  2. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

4 authors at 4 institutions in 1 country.

Chandrasekar KandaswamyAgilent Technologies, Bangalore, India.
Davis PresleyDepartment of Chemistry, Sri Sivasubramaniya Nadar College of Engineering, Chennai, 603110 India.
T P Shabeer AhammedNational Referral Laboratory, ICAR-National Research Centre for Grapes, Pune, 4123072 India.
Sreekanth AnadaramNational Institute of Technology, Trichy, India 620 015.
Agilent Technologies (India) · INNational Institute of Technology Tiruchirappalli · INNational Research Centre for Grapes · INSri Sivasubramaniya Nadar College of Engineering

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Analysis of agrochemical residues in red chilli powder is always considered difficult because of higher matrix interference due to carotenoid pigments and other co-extractives. During the sample preparation, matrix components were co-extracted along with the target compounds leading to frequent source cleaning, changing of liner and column. Efforts were made to improve the chromatographic performance by optimizing sample preparation, choosing matrix-free transitions and introducing a retention gap. The Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) extraction was experimented using different dispersive adsorbents and the purified extract was analyzed by gas chromatography tandem mass spectrometry (GC-MS/MS) system. 84 pesticides under different class were validated and established a limit of quantification of 0.002-0.007 mgkg Supplementary Information: The online version contains supplementary material available at 10.1007/s13197-021-05177-3.

Indexed as

GC–MS/MS OptimizationMultiresidue pesticidesQuEChERSRed chilliRetention gapSpices

Identifiers

PMID35531408
PMCPMC9046519
OpenAlexW3185097360

What OpenQuestion holds

Textmetadata
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.